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GC/MS analysis results for sample AD23503, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.

NYC-WTC_000088905–000088934

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088917
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23503.D Vial: 11 Acq On : 17 Oct 2001 12:01 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DAT7kBASE\NBS75K.L ********************************************************************* Peak Number 6 Oxirane, 2,3-bis(1-methylethyl- Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 29.51 2.09 ug/1 223128 Chrysene-dl2 33.12 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Oxiran^ 2,3-bis(1-methylethyl) - , t 128 C8H16O 054644-32-5 32 2 1-HepZene, 2-methyl- 112 C8H16 015870-10-7 27 3 Cyc^butane, 1,l-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 4 1-Xexene, 2-methyl- _________________ 98 C7H14 006094-02-6 27 Abundance Scan 2665 (29.510 min): 23503.D (-) Wz 56.00 100.00% 53

5000

u 41 73 257 rr, , , , , I 101 239 I _2a20_294g_2a60_2a80^_ rrr^ , , J|... I't,,, Tp-n-rp-r+ry 312 m/z SYTOO 46.31% y\fz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5067: Oxirane, 2,3-bis(1-methylethyl)-, trans- 53 41

5000 29,20 29.40 29.60 29.80 73 m/z 43.05 38.07%

Ti/z-> 20 40 J. 60 80 113128 p-T-TTyr-TTnyT-rTTp-T-Tn-^ 100 120 140 160 180 200 220 240 260 280 300 ‘ I'' ' ' I'''' I'' '' I

Abundance #64030; 1-Heptene, 2-methyl- 53

29.20 29.40 29.60 29.80 553 41 m/z 41.05 36.82%

27 I 112 pJ-p^ T I • " • I " ' ' I ' • ' ' I ’ ' ' ' I Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #21985: Cyclobutane, 1,1-dimethyl-2-octyl- ... 53 29.20 29.40 -29.60-29.80--- -m/z -5 5.-00—--31.16% 5000

27 70 I ■ ...........................................

Ti/z-> 20 40 60 . 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

23503.D NP091101.M Thu Oct 18 10:28:53 2001 Page 6

NYC-WTC_000088917

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NYC-WTC_000088917Source: NYC Law Department, mirrored locally

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