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GC/MS analysis results for sample AD23503, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.

NYC-WTC_000088905–000088934

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088918
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT1601\23503.D vial: 11 Acq On : 17 Oct 2001 12:01 am Operator: 209 GALOS- Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L

Peak Number 7 Heptadecane, 2,6,10,15-tetrame Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 29.62 0.71 ug/1 75820 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 91^ 2 Heptadecane 240 C17H36 000629-78-7 91. 3 Octadecane 254 C18H38 000593-45-3 '91' 4 Eicosane ____________________ 282 C20H42 000112-95-8 90 Abundance Scan 2677 (29.620 min); 23503. D (-) m/z 56.95 100.00% 57 43 71 85 5000

99 29.20 29.40 29.60 29.80 30.00 JU J 113 127 141 155 169 207 m/z 43.00 75.25% p n/i-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42196; Heptadecane, 2,6,10,15-tetramethyl- 57

5000 71

85 u... 29.20 29.40 29.60 29.80 30.00 m/z71.00 68.53% , , 11 , I I , , T, Tj. ..... 268, 296 ■nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71193: Heptadecane 7. ■.,i,,,,, I ,WpS /\............... 71 29.20 29.40 29.60 29.80 30.00 ■jm/z 85.05 51.70% 85

99 I J ■'2/141 155169 210 240 ............. I " ' ' I ' ' ' ' I ' ' I ' I ' ■ . I I' I . I 111 >’ I > I > ■ I I 11 I . I I I.. I I ■ I 111 I I > 11. . . I I I Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71560: Octadecane / , , 43 57 29:20 29.40 29.60 29.80 30.00- m/z—41-.05- 30.85% 71 5000 85

99 113 ■■27 141 1 169 183 197210 I'' 254 r ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80 30.00

23503.D NP091101.M Thu Oct 18 10:28:55 2001 Page 7.

NYC-WTC_000088918

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NYC-WTC_000088918Source: NYC Law Department, mirrored locally

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