GCMS analysis results for sample AD26680, Dec 10 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0401\26680.D Vial: 3 Acq On 4 Dec 2001 12:38 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise . Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Hexane, 2-methyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

10.30 1.59 ng/uL 427498 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexane, 2-methyl- 100 C7H16 000591-76-4 25 2 Hexane, 1-propoxy- 144 C9H20O 053685-78-2 25 3 Oxirane, 2-methyl-3-propyl-, cis- 100 C6H120 006124-90-9 17 4 Oxirane-;'' 2,2-dimethyl-3-propyl- 114 C7H140 017612-35-0 12 Abundance Scan 595 (10.301 min): 26680.D (-) m/ z 43.10 100.00% 43

5000

39 4 55 59

-69+4 73 85 100 J 10.00 10.20 10.40 10.60 frrrrrrr f............. .. m/z 59.10 34.87% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63434: Hexane, 2-methyl- 43

5000 10.00 10.20 10.40 10.60 57 85 29 m/z 55.10 32.50% 39

m/z-> 20 25 I m ......... ‘ TTTTTT 35 40 45 50 55 60 65 70 75 30 85 If 69 i • ■' ■ I 80 100 I " 1111111111 90 95 103 105 Abundance #8516: Hexane, 1-propoxy- 43

10.00 10.20 10.40 10.60 5000 m/z 57.10 30.87% 56 85 39 61 73 I 69 ; l • ’ " I " •11 • ’ •11 1111' TTTTTTTTTTT TTT r '" r " ■ T—‘‘1011117111-rpTrrpm- T TITTT‘I‘‘1 m/z-> Abundance i I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105

48 #1531: Oxirane, 2-methyl-3-propyl-, cis- -4 10.00 10.20 10.40 10.60 m/ z 41.10 28.41% 57 5000 71 85

100 m/z-> m 4 — TII’TTT 1TTT --*9---r4—4 'i"" i 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 10.00 10.20 10.40 10.60

26680.D NP112701.M Fri Dec 07 13:11:46 2001 Page 11

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