GCMS analysis results for sample AD26679, Dec 10 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0401\26679.D Vial: 5 Acq On 4 Dec 2001 2:27 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Hexane, 2-methyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

10.30 1.53 ng/uL 523896 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Hexane, 2-methyl- 100 C7H16 000591-76-4 17 2 Hexane, 3-ethyl-2-methyl- 128 C9H20 016789-46-1 17 3 Oxirane, 2-butyl-3-methyl- , cis- 114 C7H140 056052-93-8 17 4 Oxirane,y/2-methyl -3-propyl- , cis- 100 C6H120 006124-90-9 17 'Abundance Scan 595 (10.296 min): 26679.D (-) m/ z 43.10 100.00% 43

5000- 57 73 85 ) UN 1) > • i > • • • । ■ ■ ' ' l 1 10.00 10.20 10.40 10.60 3? + 451 — 100 1—— > . > IT . . , j , m/z 57.10 32.54% m/z--> 20 30 40 50 60 70 80 90 100 110 120 Abundance #63434: Hexane, 2-methyl- 43

5000 57 —A 10.0. 10.20 10.40 10.60 85 29 .... _ m/ z 59.10 32.36% 69 100 1 i ■ ■ ■ ' I ' 1 ' ■ i Ki i ■ ■ ■ ■ i ' ■ ■ ' i m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #5160: Hexane. 3-ethyl-2-methyl- 43 — 10.00 10.20 10.40 10.60 5000- 57 m/z 55.1.0 31.46% 1 84

m/z-> 20 27 ‘IE I i r-j > i i ! -f 30 40 II: । ■ ' ' ' । 50 60 4 70 80 90 __ 100___ 110 120 Abundance #3063: Oxirane, 2-butyl-3-methyf-, cis- —A 43 10.00 10.20 10.40 10.60 m/z 41.10 30.14% 55 5000 85 71

m/z-> ■ । ■ 20 ■ ■ ■ । 30 • r 40 1 1 i ' 1 50 ----------- 60 70 80 90 82 100 114 110 120 -- UA_ 10.00 10.20 10.40 10.60

26679.D NP112701.M Fri Dec 07 13:10:21 2001 Page 11

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