GCMS analysis results for sample AD26316, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV3 001\26316.D Vial: 27 Acq On 1 Dec 2001 11:51 am Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Hexane, 2-methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 10.32 0.43 ng/uL 214330 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexane, 2-methyl- 100 C7H16 000591-76-4 22 2 Oxirane, 2,2-dimethyl-3-propyl- 114 C7H140 017612-35-0 17 3 1-Butanol, 47( 1-methylethoxy)- 132 C7H1602 031600-69-8 12 4 Oxirane, 2-methyl-3-propyl-, cis- 100 C6H120 006124-90-9 10 Abundance Scan 598 (10.322 min): 26316.D (-) m/z 43.10 100.00% 43

5000 59 85 TUTP11 ‘ 'i 11 • ’I 73

mfc-> 20 • i ■ ■ 1 • i 1 ■ ■ • i 30 40 + TTE 50 60 1—. 470 80 90 1..... 100 110 120 m/z 10.00 10.20 10.40 10,60 59.10 44.38% Abundance #63434: Hexane, 2-methyl- 43

$ 5000 T ‘ 1 1 • ‘ * i 10.00 10.20 10.40 10.60 57 85 m/z 55.10 29 39.76% JI j | 69 , 100 fr ' r- ■ ■ i 1 1 1 1 i 1 1 ' ■ I '• 1 ‘ । ■ i • ■ •11 •1 ■111 miz-> 20 30 40 50 60 70 80। 90 100 110 120 Abundance #3003: Oxirane, 2,2-dimethyl-3-propyI- 43 59 85 -4 10.00 10.20 10.40 10.60 1 5000 m/z 57.10 33.75%

72 99 1 — 701 । — 1 114 miz—> Abundance 20 • I ' ' 1 ' I ' 1 1 ' ! 30 40 50 60

43 80 !90 #5820:1-Butanol, 4-(1-methylethoxy)- • i • ■ ■ ■ i 1 1 1 1 i 1 1 1 1 r1 100 110 120 A A 1TI 11» n 1 AUA_ 10.00 10.20 10.40 10.60 m/z 41.10 30.78% 55 73 5000

89

m/z—> ■ i ■ ■ ■ ■ i • ■ ■ ' i ■ 20 30 40 n.... 50 4 6060 —70+ 102 1 • ■ i ‘ ‘ ‘ ■ i ' • ■ ■ i 1 ‘ ‘ • I ‘ ■ • ■ i ■ 80 90 100 110 120 A

10.00 10.20 10.40 10.60 I

26316.D NP112701.M Tue Dec 04 10:12:04 2001 Page 2

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