GCMS analysis results for sample AD26316, Dec 2001

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Laboratory report documenting GCMS analysis of sample AD26316 with unidentified compounds detected.

NYC-WTC_000031262–000031273

Folder label: “GCMS X 11/3/01 A 12/1/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26316.D Vial: 27 Acq On : 1 Dec 2001 11:51 am Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.74 0.51 ng/uL 257573 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 96 2 Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 53 3 Benzofuran, 7- loro- 152 C8H5C1O 024410-55-7 9 4 Acenaphthylene 152 C12H8 000208-96-8 9 Abundance / Scan 753 (11.744 min): 26316.D (-) m/z 150.00 100.00% 150 /

5000 115 52 78 ■ — ----- ‘ ‘ I ’ * 1 ‘ 1 * 11.40 11.60 11.80 12.00

mlz-> 30 111 1 —H4040 -H 50 60 63 TTT 70 487........ 4L 80 90 100 110 120 i ■ ■ ‘ ■ i ■ ■ ■ ■ i ■ ■ 130 140 1 150 1— 160 m/z 152.00 63.87% Abundance #9593:1,4-Dichlorobenzene-d4 150

........................ ............................... 5000 115 —. . I I . i l I . . 1 . I I . . I I 1 . . 1 1 I 11.40 11.60 11.80 12.00 52 78 m/z 115.05 39.89% 87 — 35 ——— “I1 ' ’ ’ ITT i1 ■1' i ■1 ■ ■ i ■1' ■ i ‘ ‘ i. ।.... 11।. L miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150

115 11.40 11.60 11.80 12.00 5000 52 78 m/z 52.00 , 25.48%

35 87 I —........... — i'. i... ■ i.. i.. — * * ।1 * > * । * »* > । 1 '1 I' ‘'11" m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 - Abundance #10136: Benzofuran, 7-chloro- 152 11,40 11.60 11.80 12.00 m/z 78.05 24.97% 5000 89

m/z—> 35 49 * ■ i • ‘ ■ ■ i ■ • •' i ‘ 30 40 50 ' i 60 63 — 73

70 80 90 100 110 120 130 140 150 1 160 1 1 i ■ ' ' i 1 ‘ 11.40 11.60 11.80 12.00 A 26316.D NP112701.M Tue Dec 04 10:12:04 2001 Page 3

NYC-WTC_000031272

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NYC-WTC_000031272Source: NYC Law Department, mirrored locally

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