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GC/MS analysis results for sample AD23502, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23502 conducted on October 19, 2001.

NYC-WTC_000088880–000088904

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23502.D Vial: 10 Acq On : 16 Oct 2001 11:02 pm Operator: 209 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\l\METHODS\NP09il01.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Heneicosane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 34.61 2.43 ug/1 285622 Chrysene-dl2 33.13 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 9T 2 Eicosane, 7-hexyl- 366 C26H54 055333-99-8 9r 3 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 91 4 Hexatriacontane 507 C36H74 000630-06-8 91, Abundance Scan 3221 (34.613 min): 23502.D (-) m/z 57700 100760% 5|7

85 5000

I ' ' ' ' I ' 34.20 34.40 34.60 34.80 35.00 Ji, .IJ .4 ^5'* . 197 225 253 281 , |T, , . .T. I ,“i , , f. , .1 I , f, . |-, . . I I ,, . . I , . . . I , . , , I I . , , I , , , , I ., , , I , , . , I , , , , I ■m/z 71716 74.16% ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 4\bundance #42201: Heneicosane 5|7

85 n I I I r I iVi-i -| 552 I T-r-p-T 34.20 34.40 34.60 34.80 35.00 m/z 43765 67.01%

.......................I.................... ...................................................................... Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #50999: Eicosane, 7-hexyl- K 7-

XTxtlX 34.20 34.40 34.60 34.80 35.00 552 85 m/ z 85.05 50.25% A

4! 182^97 281 310 r, . jTi . . I . i7r| iV. I TjVrrfyT I' •' • f" " I " • 11 I ' ''' 1 Ti/z-> Abundance 40 60

57 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #49558: Heptadecane, 9-octyl- K T 34.20 34.40 34.60.34.80 - 35.00 “m/z 41.05----- 24-.*99%

5000 85

TiZz-> T-rp-r 40 60 XU I 239 310 . 352 i'' " I'''' I'' " I' ‘' I " '' I " " I'''' I " " I' " ' I'''' I'''' I'' " I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 34.20 34.40 34.60 34.80 35.00

23502.D NP091101.M Thu Oct 18 10:25:08 2001 Page 13 .

NYC-WTC_000088899

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NYC-WTC_000088899Source: NYC Law Department, mirrored locally

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