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GC/MS analysis results for sample AD23502, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23502 conducted on October 19, 2001.

NYC-WTC_000088880–000088904

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088897
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NYC 9/11 Public Portal Document

ribrafy Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23502.D Vial: 10 Acq On : 16 Oct 2001 11:02 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Eicosane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 32.73 2.86 ug/1 336364 Chrysene-dl2 33.13 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 91 , 2 Tetracosane 338 C24H50 000646-31-1 93?> 3 Heneicosane 296 C21H44 000629-94-7 91 /. 4 Octadecane ___________________________ 254 C18H38 000593-45-3 91/ Abundance Scan 3016 (32,731 min): 23502,D (-) rnT^ 57700 107700% 5f7

85 5000 /... ,R...... Ti/2-> Abundance iU ,1, jl. ■'’r.,/ ,19/ ,225 253 281 . 111, q , Ir, 111.. f 111111 r11 |-i 11 r 1, 111111.11 ■ 111111 < 111 ■ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #39862: Eicosane T 352 '''' I 32,40 32,60 32,80 33,00 m/z 71.10 I 71753%

57

85 V 553 ■ T' ' ' I I ' I ' I I 32,40 32,60 32,80 33,00 m/z 43.05 77741%

m/z-> 40 " I'' 60 196 240 282 '' I'''' I'''' I'''' I'''' I'''' I'''' I'''' I'''' I'''' I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 A Abundance #73543: Tetracosane 57

' ' I 32.40 32.60 32,80 33,00 5000 85 m/z 85.05 50.54% *

m/z-> JU 'I'' " p 155 183 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 294 338

Abundance #42201: Heneicosane 57 32,40 32,60 32,80 33,00 Wz 41..05 25.76% 85 5000

I 113 TT-p-r I f fj, t r I rr>i-r TlZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32,40 32,60 32,80 33,00

23502.D NP091101.M Thu Oct 18 10:25:03 2001. Page 11

NYC-WTC_0000888‘97

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NYC-WTC_000088897Source: NYC Law Department, mirrored locally

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