GC/MS analysis results for sample AD23473, Oct 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23473.D Vial: 4 Acq On : 16 Oct 2001 5:10 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Tetracosane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 31.73 4.81 ug/1 558243 Chrysene-dl2 33.12 Hit# Of 5 Tentative ID MW MolForm CAS# Qual yl^etracosane 338 C24H50 000646-31-1 96 2^Eicosane 282 C20H42 000112-95-8 91 3 Octadecane 254 C18H38 000593-45-3 91 4 Heneicosane _________ .__________ 296 C21H44 - 000629-94-7 91 Abundance Scan 2908 (31.735 min): 23473.D (-) m/z SYTOO 100.00% 57 43 71

5000 85

I ^113 M[....... 31.40 31.60 31.80 32.00 .1 i. JI, J j 83197211225239253267281 338 I 1 'p I I'T] I n I prI I r| I iTj j I I ■ > (< 'rtV। । r । । i”! । । r । m ■ । i । । ■ i ■ । ■ ■ ■ i i't i ■ ■ । ■ i '' I'''' I'' m/z 71.00 72.60% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 71

5000- 85 r' ' T T 31.40 31.60 31.80 32.00 99 m/z 43705 70714% I , il \'j3l27 155169183197 294 338 '' I ’''' I'''' r ''' I'' ’' I'''' 1'' Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #39862: Eicosane,__ ‘ 43 S|7' 71 31.40 31.60 31.80 32.00 5000- 85 m/z 85.00 49744% (1 I 113127141155 196 240 282

Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance 57 #71561: Octadecane A 31.40 31.60 31.80 32.00 .. r 43 71 " ' m/z 41.05 27.17% 5000 85 A

n/z-> 40 60 l| 99 J 224 254 ‘ r ''' r * *' I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 /vUt 31.40 31.60 31.80 32.00

23473.D NP091101.M Wed Oct 17 13:17:44 2001 Page 11

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