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GC/MS analysis results for sample AD23473, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.

NYC-WTC_000088725–000088752

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088741
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NYC 9/11 Public Portal Document

LibrarySearch Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23473.D Vial: 4 Acq On : 16 Oct 2001 5:10 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L * * * * *■* ********************* * * *************************************.^*.A.

Peak Number 10 Butyl tetradecanoate (myristat Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 31.64 3.75 ug/1 434608 Chrysene-dl2 33.12 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

VJer'Butyl tetradecanoate (myristate) 284 C18H36O2; 000000-00-0 80 2 Oxirane, 2,3-bis(1-methylethyl)-, t 128 C8H16O 054644-32-5 32 3 Cyclohexane, (1,1-dimethylethyl)- 140 C10H20 003178-22-1 27 4 Cyclobutane, l-hexyl-2,3-dimethyl- 168 C12H24 055170-84-8 25 'Kbundance Scan 2898 (31.643 min): 23473.D (-) m/z 56.00 100.00% 53

553 4' 73 129 285 / \A f ' ' ’ '7 I 97 I , 157 . 213 241 267 j 31.40 31.60 31.80 32.00 340 m/z 57700 49.00% Abundance 20 40

53 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #40186: Butyl tetradecanoate (myristate) fl 5000 229 31.40 31.60 31.80 32.00

Tife-> Abundance 20 40 u 60 __ 73 129 ...... 211

I' ' '' I '' ' ' I' ' '' I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #5067: Oxirane, 2,3-bis{1-methylethyl)-, trans- p-m-j- 284 ■ 11" ’ I' I " 11''' I

____ ___ m/z; 43.05 39.43%

41 53 ffi _31jg_3t60_3t80_jzog_ m/z 41705 35.13% 5000

73 113128 -m-p-m I'''' I'''' I'''' I'''' I ■nfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #7604: Cycloh^ne, (1_,1-dim^ylethyl)-_ _ ' I-' 31.40 31.60- 31:80 : 32.00 - m/z 73.00 29.36%

5000 41

82 I I 125140 ' " I' ‘ " I -y+n-rp-m-p I'''' I'''' I'' ’' I'''' r ''' I'''' I' ‘' I T TiZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23473.D NP091101.M Wed Oct 17 13:17:42 2001 Page 10

NYC-WTC_000088741

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NYC-WTC_000088741Source: NYC Law Department, mirrored locally

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