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GC/MS analysis results for sample AD23473, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.

NYC-WTC_000088725–000088752

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088740
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23473.D vial: 4 Acq On : 16 Oct 2001 5:10 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L Peak Number 9 Tricosane Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 30.70 2.50 ug/1 290392 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolFoirm CAS# Qual

Tricosane 324 C23H48 000638-67-5 93 2 Eicosane 282 C20H42 000112-95-8 91 3 Tetracosane 338 C24H50 000646-31-1 91 4 Heneicosane 296 C21H44 000629-94-7 91 Abundance Scan 2795 (30.697 min): 23473. D (-) m/z 56.95 100.00%! 43 57 71 fl 5000 85

■n/z-> Abundance 40

43 57 u 60 99 .1 J T^?^1^^1551^183197211225 253___________ 324 •Tph-rlYrTTTp-VTTfTTTV-p-l'T-rj-rTTTp-rTTpn-rTp-rTTyTT-rTpT-TTp-r^^ 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #73318: Tricosane y L I ' ' ' ' I 30.40 30.60 30.80 31.00 m/z 71.00 71713%

71 5000 85 -7 L. ■p-’T-T-T-p T 30.40 30.60 30.80 31.00 m/z iTToy; 70.89% I I T’P'th’ 183197211225 ' r* ‘I'' ' I ' p"''' I 296 324 " • I " «' I ‘ ' I' TT^-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #39862; Eicosane ________ _ __ 4? 71 I"'' '^r'’' I' I 30,40 30.60 30.80 31.00 5000- 85 m/z85.05 47.27%

pn^Tq-^^rTTYrT+Tp-¥TTYTnrTVp-rrTpTn-TpnTTyTTTTq~rTTTprTTTjSTTTJTTTT-p-^^ TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 flibundance #73543; Tetracosane 43 57 - . 30.40 30.60 30.80 31.00 71 m/z 41705 29.75% 5000- 85

155169183197 294 338 P" I ' ' ’' I T^ I ' I ' ' ' ' P ‘ ’I -rrry 9^' Tl/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 30.40 30.60 30.80 31.00

23473.D NP091101.M Wed Oct 17 13:17:40 2001 Page 9

NYC-WTC_000088740

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NYC-WTC_000088740Source: NYC Law Department, mirrored locally

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