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GC/MS analysis results for sample AD22654, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22654 conducted on October 12, 2001, noting other unknown compounds.

NYC-WTC_000087463–000087490

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087478
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NYC 9/11 Public Portal Document

Library Search Compound Report • Data File : C:\HPCHEM\1\DATA\OCT1101\22654.D Vial: 6 Acq On : 11 Oct 2001 2:38 pm Operator: 209 GALOS Sample : reinject Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L

Peak Number 7 1-Nonadecanol Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 29.75 0.89 ug/1 138307 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual CU 1-Nonadecanol 284 C19H40O 001454-84-8 93 2 1-Octadecanol 270 C18H38O 000112-92-5 81 3 1-Heptadecanol 256 C17H36O 001454-85-9 81 4 4-Tetradecanol 214 C14H30O 001653-33-4 81 Abundance Scan 2691 (29.748 min): 22654.D (-) m/z 1^3.05 100.00% 43

” 69 “ 5000 97 111 luU I r. I . J I I I . I

n/z-> mt jLUX-Xjx- 60 80 100 120 140 160 180 200 207 224 220 240 29.40 29.60 29.80 30.00 m/z 83.00 60.21% Abundance #40236:1-Nonadecanol 55

Ui 83 69 97

5000 XI" ' 111 29.40 29.60 29.80 30.00

Ti/z-> ^bundance 31 42

11 ' ' ' I ' ' 40 II Xl 60 80 100 125

120 ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' 140 #72028:1-Octadecanol 160 180 200 220 238 240 m/z 57100 57117%

57 69 8? 97 Ji A *^1 29.40 29.60 29.80 30.00 m/z 60195 51.04% 5000 111

■n/z-> Abundance ' I ' ' ' 40 60 I ' ' ' I ' 80 Ux 100 125

120 140 153 ' ' I ' ' 140 #35210:1-Heptadecanol ' I ' ' ' ' I ' ' ' ' I ■ 160 180 200 224 220 ' 240 . 1,J\. . 55 29,40 29.60 29,80 30.00 69 83 m/z 69.00 50.89% 97 5000 111 125

■n/z-> 40 60 I ' ' ' ' I 80 ji U l .... 210....238 100 120 140 160 180 200 220 240 ' ‘ ' I ' ' ' ' I 29,40 2a60 2a80 3a00

22654.D NP091101.M Fri Oct 12 09:09:17 2001 Page 7

NYC-WTC_000087478

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NYC-WTC_000087478Source: NYC Law Department, mirrored locally

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