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GC/MS analysis results for sample AD22654, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22654 conducted on October 12, 2001, noting other unknown compounds.

NYC-WTC_000087463–000087490

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087479
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NYC 9/11 Public Portal Document

Library Search Compound Report ■ Data File : C:\HPCHEM\1\DATA\OCT1101\22654. D Vial; 6 Acq On ; 11 Oct 2001 2:38 pm Operator: 209 GALOS Sample : reinject Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Tricosane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 30.70 2.74 ug/1 424484 Chrysene-dl2 33.13 JUt# Of 5 Tentative ID MW MolForm CAS# Qual /Tricosane 324 C23H48 000638-67-5 97 Heptadecane 240 C17H36 000629-78-7 91 3 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 91 4 Octadecane 254 C18H38 000593-45-3 90 Abundance Scan 2795 (30.702 min); 22654. D (-) m/z 57700 107700% 43 7 71 (1 5000 85 ■L I 99 30.40 30.60 30.80 31.00 . ,;'i. .I‘|, ,'K, ‘ '1 ' 324 ' I ‘ ' m/z 71.00 71.44% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #73318; Tricosane 4(3 57

71 5000 85 xLL I ~ I T 30,40 30.60 30.80 31.00 m/ Z 43.05 67.89% I I 99 113127141 183197211225 296 324 “T I ' • •' I '' ‘' I • •'' p '' ' I ’' • t p ' ’ IJ ■nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #71193; Heptadecane 57

71 1 30.40 30.60 30.80 31.00 m/z 85.05 47.79% 5000 85

99 J ^P''?7141 155169 210 240 ■rYrriH-y-rVr-r-[‘T-T-^^ T ''' ' I''' ' I'' 11 • I»I' '' i pt' ’ I m/z-> ^bundance 40 60

7 80 100 120 140 160 180 200 220 240 260 280 300 320 #42196; Heptadecane, 2,6,10,15-tetramethyl- A 30.40 30.60 30.80 31.00 71 m/z 41.00 27777% 5000 85 J

■n/z-> 40 60 X 80 183 211 100 120 140 160 180 200 220 240 260 280 300 320 268 296 1''''I'''‘I' J I ' ' ' 30.40 30.60 30.80 31.00

22654.D NP091101.M Fri Oct 12 09:09:19 2001 Page 8

NYC-WTC_000087479

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NYC-WTC_000087479Source: NYC Law Department, mirrored locally

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