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GC/MS analysis results for sample AD22654, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22654 conducted on October 12, 2001, noting other unknown compounds.

NYC-WTC_000087463–000087490

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087480
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NYC 9/11 Public Portal Document

Library Search Compound Report • Data File C:\HPCHEM\1\DATA\OCT1101\22654.D Vial: 6 Acq On : 11 Oct 2001 2:38 pm Operator: 209 GALOS Sample : reinject Inst ; GC/MS 209 Mise Multiplr: 1,00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L

Peak Number 9 Butyl tetradecanoate (myristat Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 31.64 4.77 ug/1 740272 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual

T Butyl tetradecanoate (myristate) 284 C18H36O2: 000000-00-0 80 2 Octadecanoic acid, butyl ester 340 C22H44O2; 000123-95-5 39 3 Decane, 2,2,3-trimethyl- 184 C13H28 062338-09-4 35 4Cyclobutane,l,l-dimethyl-2-octyl- 196 C14H28 062338-30-1 35 Abundance Scan 2897 (31.639 min): 22654.D (-) m/z 56.00 100.00% 5b

aaS 4 73 ;-V\ , ...... ' ' ' ' I ' I ' ' 340 __3L4p_3t60_^L8p_JZ00_ m7z 57.00 50.84% Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate)

5000 I 'I I i-rr 229 31.40 31.60 31.80 32.00 73 211 m/z 43 ;oo 39.67% 129 284 111" 1111111 ■ 1111 yTTrrytTTTYTT^'rYT-m-^^ Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73570: Octadecanoic acid, butyl ester 55

31.40 31.60 31.80 32.00 5000 m/z 41.05 37.00% 285 340

^bundance 20 Ju 129 185 l 267

rrpn-TTyrrT-ryTTT 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #19005; Decane, 2,2,3-trimethyl- ..... UL.... 7 31.40 31.60 31.80 32.00 m/z 73.00 30.30% 550

1J y, ................. nZz~> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

22654.D NP091101.M Fri Oct 12 09:09:21 2001 Page 9

NYC-WTC_000087480

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NYC-WTC_000087480Source: NYC Law Department, mirrored locally

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