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GC/MS analysis report for sample AD22544, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22544 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086913–000086932

Folder label: “508 Scan 9/17/01 9/26/01

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Scanned page image, NYC-WTC_000086925
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C;\HPCHEM\l\DATA\SEP2501\22544.D Vial: 10 Acq On : 25 Sep 2001 11:15 pm Operator;. 2 09 GALOS Sample ; GC/MS unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L ************************************************************************ Peak Number 4 Pentadecane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 31.77 0.40 ug/1 50792 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual

Pentadecane 212 C15H32 000629-62-9 90 2 Tridecane, 1-iodo- 310 C13H27I 035599-77-0 86 3 Pentacosane 352 C25H52 000629-99-2 86 4 Tetradecane 198 C14H30 000629-59-4 86 Abundance Scan 2912 (31.771 min): 22544.D (-) Wz 57700 100.00% 57

71

JI 43 5000 85

t 31 40 31.60 31.80 32.00 32.20 209 281 '' I ’'' ' I ''' ' I' '' ■ I'' '' I '' '' I ''' ' I' ' m/z 71.00 65.80% •n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #70273: Pentadecane 43 5)7

71 5000 85 I ' ' ' ' I T 31 40 31,60 31.80 32.00 32.20 27 Wz 43.05 59.84% 1?127141 170 212 J ' I ' ' ' ' I ‘ ' I ' ‘ ‘ ' I ' ' ' ' I I ' ' ’' I ' ' ' ' 1 ' ' ' • I n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44187: Tridecane, 1-iodo- 5)7 43 71 31 40 31.60 31.80 32.00 32.20 5000 85 m/z 85705 47.86%

183 I 310 I ''' ' I' ■nfe--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #73718: Pentacosane A 4)3 5,7 31 40 31.60 31.80 32.00 32.20 m/z 55.00 23.34% 71 So, 85

....... I ,, [ I, t,, T J69183197211225............................. ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 31.40 31.60 31.80 32.00 32.20

22544.D NP091101.M Mon Oct 01 12:59:06 2001 Page 4

NYC-WTC_000086925

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NYC-WTC_000086925Source: NYC Law Department, mirrored locally

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