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GC/MS analysis report for sample AD22544, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22544 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086913–000086932

Folder label: “508 Scan 9/17/01 9/26/01

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Scanned page image, NYC-WTC_000086924
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2501\22544.D Vial: 10 Acq On : 25 Sep 2001 11:15 pm Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ******★****************'********************************************** Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 11.65 0.53 ug/1 63800 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 1,4-DicJa<lorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 35 3 Benzeniamine, 2-methyl-4-nitro- 152 C7H8N2O2 000099-52-5 12 4 Beggenamine, 2-methyl-5-nitro- 152 C7H8N2O2 _______ 000099-55-8 10 4bundanc< Scan 720 (11.647 min): 22544. D (-) m/z 149.90 ,100.00% 1!i0

5000

52 78 115 L T-p-T 11.40 11.60 11.80 12.00 40 4^ m/z 151.90 64.95% 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593; 1,4-Dichlorobenzene-d4 1!i0

5000 52 78 115 Jy 11.40 11.60 11.80 12.00 m/z 114.90 . 32.74% 35 ....... ■n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592; Benzene-1,2,3,4-d4-, 5,6-dichloro- 1!i0

115 11.40 11.60 11.80 12.00 5000- 52 78 Wz 78.05 . 19.70%

35 87 I 1 ■n/z-> Abundance ' I ‘ 30 ' I ' ' ' ' I 40 50 ' ' ' I ' ' ' * I ' 60 70 80 90 100 110 120 130 #10129: Benzenamine, 2-methyl-4-nitro- 77 106 140 150

152 160 T T L 11.40 11.60 11.80 12.00 m/z 52.00 15.45%

55® 51 94 66 I m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.40 11.60 11.80 12.00

22544.D NP091101.M Mon Oct 01 12:59:04 2001 Page 3

NYC-WTC_000086924

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NYC-WTC_000086924Source: NYC Law Department, mirrored locally

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