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GC/MS analysis results for sample AD23322, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23322 conducted on October 15, 2001.

NYC-WTC_000088263–000088289

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088280
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23322.D Vial: 15 Acq On : 12 Oct 2001 3:48 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209' Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Tetracosane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 31.73 4.11 ug/1 428389 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

Tetracosane 338 C24H50 000646-31-1 99 Heneicosane 296 C21H44 000629-94-7 91 3 Heptadecane 240 C17H36 000629-78-7 91 4 Eicosane ____________________ 282 C20H42 000112-95-8 91 ^bu^dance Scan 2908 (31.734 min): 23322.D (-) m/z 57.00 100.00% 57 71 43 85

I tt/z-> ^bundance u40 I i J, iJ 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #73543: Tetracosane 338 T-ry 31.40 31.60 31.80 32.00 ■m/z 71.00 72.50%

43 5 7 71

5000 85 M 31.40 31.60 31.80 32.00 m/z 43.05 65.46%

•n/z-> 40 JJJteL 155169183197 I I I . I I T , , . I , , 60 , I I 1 I . I I ’ ‘ ’ I 294 r ''' I'''' I ‘' I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 338 I''' ' I ' J Abundance #42201: Heneicosane 57 71 ul 1 ' ' ' ' 31.40 31.60 31.80 32.00 85 5000 m/z 85.00 50.23%

99

'' I ’' pnH-TT-ThnTY^T-TTyTrTTYTTTVp-TT-TyTTTTpT-rryT-nny^ .............. ■nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance 5^ #71193: Heptadecane M 31.40 31.60 31.80 32.00 T m/z 41.05 27.05% 71 5000 85

99 ............ ;........................ J ^P1?7141155169 210 240 T^rT¥yTT+Tp*TTfTTTTTrTTTT I'''' I'''' I'' I'''' I'''' I'''' I'''' I ■nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23322.D NP091101.M Mon Oct 15 10:26:10 2001 Page 11

NYC-WTC‘_000088280

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NYC-WTC_000088280Source: NYC Law Department, mirrored locally

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