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GC/MS analysis results for sample AD23322, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23322 conducted on October 15, 2001.

NYC-WTC_000088263–000088289

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088281
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HP’CHEM\1\DATA\OCT1201\23322 .D Vial: 15 Acq On : 12 Oct 2001 3:48 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L Peak Number 12 Tetracosane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 32.73 3.89 ug/1 405997 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane 338 C24H50 000646-31-1 9(k 2 Eicosane 282 C20H42 000112-95-8 90 2 3 Octadecane 254 C18H38 000593-45-3 87/ 4 Heptadecane 240 C17H36 000629-78-7 87' Abundance Scan 3016 (32.726 min): 23322.D (-) Wz 57.00 100.00% 57 71 43 5000 85

99 .JX I ' 32.40 32.60 32.80 33.00 ' I

■•i'i., l‘i . ||'I| ■ ■ I ' ' ' ' I m/z 71.10 70.75% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 5(7 71

552 85 32.40 32.60 32.80 33.00 99 m/z 43.05 63.87% l| 155169183197 294 I'''' I'I I ' I I > ■ ' I ' ' ' ' I ' ‘ 1’1 ' I 'i I I ■’! I I I , I > > • • I , ' • ' I ' ' " I ' " ' I 338 ■pnrrrp- ■nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance #72326: Eicosane 57 43 71 32.40 32.60 32.80 33.00 5000 m/z 85.05 49.76% 85 fl 99 J I]3i27i41155169 282 ■I ‘'r«1'''' f'''' I'''' I I ' ' ' ' I 1 (1111111111 Ti/z-> 40 60 80 100 120' 140 160 180 200 220 240 260 280 300 320 340 Abundance #71560: Octadecane 7 43 57 32.40 32.60 32.80 33.00 m/z 41.05 27774% 71 5000 85

99 254 '' ' I ' i ' ' ’' p ' ' ' I ’ ' '' J • ' I ‘ I ' I ' ' ' ' I ' ' ' ' I V Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00

23322.D NP091101.M Mon Oct 15 10:26:12 2001 Page 12

NYC-WTC_000088281

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NYC-WTC_000088281Source: NYC Law Department, mirrored locally

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