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GC/MS calibration data for TCLP method, Oct 2001

Machine-extracted title · confidence 100%

Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.

NYC-WTC_000087496–000087516

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT0201\LB.D Vial: 2 Acq On ; 2 Oct 2001 3:06 pm Operator; 2 09 G7\LOS Sample : 9/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ' : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Pentacosane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 33.72 1.45 ug/1 221588 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentacosane 352 C25H52 000629-99-2 91 2 Heneicosane 296 C21H44 000629-94-7 91 3 Tetracosane 338 C24H50 000646-31-1 91 4 Tricosane 324 C23H48 000638-67-5 91 Abundance Scan 3124 (33.717 min): LB.D (-) m/z 57.00 100.00% 5|7 71 43

5000- 85

T T ' 1 ' ' ' ' I 33.40 33.60 33.80 34.00 , r,, ..... ,,,,,,, m/z 71.00 72.14% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 <\bundance #73718: Pentacosane 43 57

71 5000- ----- i-rf> ri |-|-| < I -rYr I r I I r I I I I 85 33.40 33.60 33.80 34.00 m/z 43.05 65.45% "I pi 27141155169183197211225 '' I' tJU -T’YrTTHqp-HT-jhrTTyp-rTTpTTTYr^^ I'' ‘' I' • " I' ” J ■nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 /\bundance #42201: Heneicosane 57 J V 71 T'''' r T 85 33.40 33.60 33,80 34.00 5000 m/z 85.05 49.32%

Ti/z-> Abundance 40 44 60 80 a 99 127141155 pn-rrp-rrrpnTnyrTTTyTTTTy I' ‘ " I " '' I 268 100 120'140 160 180 200 220 240 260 280 300 320 340 #73543: Tetracosane 296

' •^1 ' I 43 5t7 33.40 33.60 33.80 34.00 71 m/z 41.00 25.04%

5000- 85

l| 155169183197 294 338 ’ ' ' I I' '' ' I I " '' I I''' ‘ I " •' I'' I' I I''' ’T* ttZ2-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 33.40 33.60 33.80 34.00

LB.D NP091101.M Wed Oct 03 10:10:06 2001 Page 11

NYC-WTC_000087512

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