GCMS analytical results for sample AE03825, March 29, 2002

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Data File : C:\HPCHEM\1\DATA\MAR2 20 2\3 8 2 5.D Vial: 6 Acq On : 22 Mar 2002 11:03 pm Operator: Sample : gc/ms scan 2/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ****************************************** * * * ** ******* * * * * * ********** Peak Number 1 1-Monolinoleoylglycerol trimet Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

37.39 0.41 ug/1 31734 Perylene-dl2 37.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoyl glycerol trimethylsi 498 C27H54O4Si2 054284-45-6 25 2 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 12 3 Benzoic acid, /2 ,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 9 4 2-Propenamide, • 3-(4-hydroxyphenyl) - 283 C17H17NO3 020375-37-5 7 Abundance Scan 3524 (37.395 min): 3825.D (-) m/z 73.00 100.00% 73 147 5000- 221 355 281 429 49

mlz-> — 50 i 191 — 2531 Il l 327 ---------------- 37.00 37.20 37.40 37.60 37.80 m/z 146.95 53.39% 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000- 147 —AA-AAMM-AWMAAAA I 37.00 37.20 37.40 37.60 37.80 34 I 103 ............ .................. m/z 221.05 | 46.83%

m/z-> 50 100 150 200 250350 400 300 450 — 325, 500 2550 Abundance #60503: 3-lscDropoxv-1.1.1.7.7.7-hexamethyl-3.5.5-tris(trirn 73 i ■ ■ ' ■ i ' ■ T-r-j-r-r-T-r-j-T-r 37.00 37.20 37.40 37.60 37.80 5000 m/z 207.00 3 4.22% 147 Aww wwywww -..................... 21.2 327......... 415........... 519 , 561 m/z-> 50 100 150 20 250 300 350 400 450 500 550 Abundance #51296: Benzoic acid, 2,6-bis((trimethylsilyl)oxy]-, trimet 73 ' 355 37.00 37.20 37.40 37.60 37.80 27.40% 5000

147 267

m/z- 47 — 208.237 A , I ' ' ' ■ i ' ' 1... f 1 1 I ’ 11 > I ' 1 50 100 150 200 250 300 350 400 450 500 550 37.00 37.20 37.40 37.60 37.80

3825.D GCMS0308.M Tue Mar 26 14:54:31 2002 Page 1

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