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GCMS analytical results for sample AE03825, March 29, 2002

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Laboratory report listing detection results for volatile organic compounds in sample AE03825 analyzed on March 29, 2002.

NYC-WTC_000038032–000038041

Folder label: “GCMS X 2/20/02 A 3/22/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2202\3825.D . Vial: 6 Acq On : 22 Mar 2002 11:03 pm Operator: Sample : gc/ms scan 2/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 3-(3-Hydroxyphenyl)-3-hydroxyp Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

38.85 0.47 ug/1 36441 Perylene-dl2 37.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-(3-Hydroxyphenyl)-/-hydroxypropio 398 C18H3404Si3 000000-00-0 10 2 2-Propenoic acid, [2-(4-chlorophe 265 C12H8C1NO2S 021278-79-5 9 3 N-Phenylacetyl glycine, trimethylsi 265 C13H19NO3Si 000000-00-0 9 4 3-Isopropoxy-1,1/1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 9 Abundance lean 3683 (38.854 min): 3825.D (-) m/ z 73.00 100.00% 73

147 5000 221 281 355 ' ■ i ■ ■ ■ ■ i ■ ' 429 38.60 38.80 39.00 39.20

m/z-> 44 T’TTTT — I T 193 ।

20 40 60 80 100120140160180200220 240260280 300 320 340 360 380400 420 m L 11' " I m/z 147.00 59.78% Abundance #53668: 3-(3-Hydroxyphenyl)-3-hydroxypropionic acid, tri-TMS 73 267

5000 147 ■ Ju Ad AM4 M ,,, WAA M A 38.60 38.80 39.00 39.20

A 207 398 m/z 221.05 ' 39.49% 47 293 341 TTTT l1»’ • i * * > • । •i i ""i"" i" *'i ""i" "I ‘T T TTT TT.... m/z-> 20 40 60 80 100120140160180200220240260 280 300 320 340 360 380400420 Abundance #36709: 2-Propenoic acid, 3-12-(4-chlorophenyl)-4-thiazoly 39 221 84 265 38.60 38.80 39.00 39.20 5000 m/z 281.00 27.62% I 111

....... I... ;.. 138 ।।P... P।।। >.>>।।।। > 11.... 1111111111111111 ~wMyw WwA m/z-> 20 40 60 80 100120140160180200220240260 280 300320 340 360 380 400 420 Abundance #36723: N-Phenylacetyl glycine, trimethylsilyl- 73 38.60 38.80 39.00 39.20 m/z 355.15 27.06% 5000 .

30 92 1)8 174 221 250 _ I I 1 148 174 IE‘ITEEIEITTETEICETTTTTTTT ‘I‘TITEI‘‘T I ""I 1 1 II I ""I"" I"" I"" I" "I m/z-> 20 40 60 80 100 120 140160 180 200 220 240 260 280 300 320 340 360 380 400 420 38.60 38.80 39.00 39.20

3825.D GCMS0308.M Tue Mar 26 14:54:36 2002 Page 2

NYC-WTC_000038040

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NYC-WTC_000038040Source: NYC Law Department, mirrored locally

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