Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30650.D Vial: 46 Acq On : 30 Dec 2001 3:26 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 3-(3-Hydroxyphenyl)-3-hydroxyp Concentration Rank 13
R.T. EstConc Area Relative to ISTD R.T.
36.71 0.59 ug/1 161703 Perylene-dl2 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-(3-Hydroxyphenyl)-3-hydroxypropio 398 C18H3404Si3 000000-00-0 38 2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 3 Trisiloxane, 1,1, 1,5,5,5-hexamethyl 3 84 C12H3 604Si5 003555-47-3 32 4 2-Butenoic a bid, 3-methyl-2-[(trime 260 CllH24O3Si2 055044-79-6 72.95 100.00% 32 'Abundance Scan 3449 (36.709 min): 30650.D (-) m/z 73
147 5000 221
! 41 96 117 l 193 . 240 281 .. 327 , 355 1 401 0 439 36.40 36.60 36.80 37.00 '" (i ■. n ■ il 11 chi " ■' । ■' TMTTTTHT TITT m/z 147.00 53.56% m/z-> 40 60 80 100 120140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #53668: 3-(3-Hydroxyphenyl)-3-hydroxypropionic acid, tri-TMS 73 267
5000 147 Di M -rr 2IIIIT7 Pa shorm 36.40 36.60 36.80 37.00 207 398 29.77% 47 j *umumm)umpmmPTpTm T‘293 341—00001031—, 9221030010131303 1—011001111 m/z-> 40 60 80 100120140160180 200 220 240260280 300 320 340 360 380400420 Abundance 71003 Ehanedioe acid, bisttrimettiisiivij ester 73
147 36.40 36.60 36.80 37.00 5000 m/z 207.00 17.63% 45 117 190 219 wAkoyko SyAAW h m/z-> 40 60 80 100120140160180200 220 240 260 280 300 320 340 360 380400420..... Abundance। #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 36.40 36.60 36.80 37.00 147 m/z 281.00 16.14% 5000 281 45 369 .... d......... 117.... .... TIT—207 10111011310111115313100010000111T 249—uu mu!m I ; —muang I , m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 36.40 36.60 36.80 37.00
30650.D GCMS1126.M Mon Jan 28 11:19:06 2002 Page 15
NYC-WTC_000004385
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Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
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Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
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Laboratory report detailing GCMS analysis of sample AD28271 conducted on December 6, 2001.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
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