Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.
NYC-WTC_000088905–000088934Folder label: “GC/MS Scan 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23503.D Vial: 11 Acq On : 17 Oct 2001 12:01 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 18 Trisiloxane,■ 1,1,1,5,5,5-hexam Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 41.72 4.26 ug/1 405945 Perylene-dl2 37.23
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxan^ 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 37 2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 27 3 3,6-Dio:^-2,4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 25 4 Mercapt/Sacetic acid, bis (trimethyls 236 C8H20O2SSi2 006398-62-5 23 Abundance Scan 3995 (41.720 min): 23503.D (-) jn/z 73.00 100.00% 147 221 5000 281 355 I ' ' ' ' I ' ' ' ' I 429 41.40 41.60 41.80 42.00 44 117 , 327 L rl+r "t " '| "T'l .I , .j., .T|... 11.... i'.. m/z 147.00 77710% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 7(3 147
5000 41.40 41.60 4l!b0 42'00 ' ' 281 m/z 221.05 55.48% 45 369 I , I “ "I 117 207 249 ............ L.............. p •" I" " I' •. 11 "“11111111111.111" 11 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #71006: Ethanedioic acid, bis(trimethylsilyl) ester -73 ................. ,-1 147 41.40 41.60 41.80 42.00 5000 m/z 281.00 30.88%
45 I I I'"' I”'' I ...7/.-.,.I... 190 219 rTTkTT-rVTTATTTT4TTTTTTTTT-rTTTTTTTT=^T-rTTTT-rTT^^ |TTTTpTTTpTTTpTTTp-rTTpTTTpTTTpTrrpTTTJT^ mfe-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 1 17 Z!1- 41,40 41.60-41.80-42.00 m/z ^55.05 -- 23-. 7^ 73 ssa 117 191
L 279 TTTrrp-rrJfTTTTp-rTTjTTTrpTr^^ __ /..\sr.. I • ’' * I ■n" m/2-> 40 60 80 100120140160180200220240260280300 320340360380400420 . 41.40 41.60 41.80 42.00
23503.D NP091101.M Thu Oct 18 10:29:20 2001 Page 18
NYC-WTC_000088929
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NYC-WTC_000087274
Laboratory report documenting GC/MS analysis of sample AD22652 conducted on October 11, 2001, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088725
Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088207
Laboratory report documenting GC/MS analysis of sample AD23320 conducted on October 15, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088346
Laboratory report documenting GC/MS analysis of environmental sample AD23270 conducted on October 15, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089418
Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088263
Laboratory report documenting GC/MS analysis of sample AD23322 conducted on October 15, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088853
Laboratory report documenting GC/MS analysis of sample AD23501 conducted on October 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088456
Laboratory report documenting GC/MS analysis of environmental sample AD23272 conducted on October 15, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088556
Laboratory report documenting GC/MS analysis of environmental sample AD23345 conducted on October 16, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088372
Laboratory report documenting GC/MS analysis of environmental sample AD23271 conducted on October 15, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089476
Laboratory report documenting GC/MS analysis of sample AD23834 conducted on November 1, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088316
Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000088695
Gas chromatography-mass spectrometry scan results recorded on September 27, 2001 for environmental samples.
Filed in the same folder
NYC-WTC_000088696
Fragmented GC/MS scan page from a laboratory blank sample dated September 27, 2001.
Filed in the same folder
NYC-WTC_000088700
Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
Filed in the same folder
NYC-WTC_000088725
Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.
Filed in the same folder
NYC-WTC_000088753
Laboratory report documenting GC/MS analysis of sample AD23497 conducted on October 19, 2001.
Filed in the same folder