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GC/MS calibration data for sample 30643, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018445–000018469

Folder label: “GCMS X 12/18/01 A 12/30/01

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Scanned page image, NYC-WTC_000018467
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\30643.D Vial: 59 Acq On : 30 Dec 2001 5:02 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 17 Ethanedioic acid, bis(trimethy Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 36.72 1.40 ug/1 415732 Perylene-dl2 37.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethanedioic acid, bis(tri thylsily 234 C8H1804Si2 018294-04-7 38 2 Mercaptoacetic acid, bis rimethyls 236 C8H20O2SSi2 006398-62-5 28 3 1,2-Benzenedicarboxyli acid, bis(t 310 C14H2204Si2 002078-22-0 25 4 Propanoic acid, 2-oxo -(trimethyls 232 C9H20O3Si2 055887-51-9 23 Abundance Scan 3450 (36.715 mln): 30643.D (-) m/z " 73

147 5000 221 281 355 401 429 36.40 36.60 36.80 37.00 . 45 „ 117 . Onuaseiryainnmph , S94 191 L , 249 327 ‘ I TpTHTT mmpmntm T uTimyrmipe m/z 147.10 59.07% mlz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #710)6: Ethanedioic add, bis(trlmethylsilyl) ester 73 147 5000 ==TI=n—Rmp 36.40 36.60 36.80 37.00 45 m/z 221.05 36.37% ................... 117190 219 ...... ......................... m/z-> 40 60 80 100 120 140 160180 200220 240 260 280 300 320 340 360 380 400420 ‘ Abundance #30949; Mercaptoacetic acid, bis(trimethylsilyl)- 73 147 I BBBngn" ! I I’l’l ’1 I "I’Tl T 36.40 36.60 36.80 37.00 5000 m/z 281.00 18.43% 221 45 1104 I 193 11.. I n.. j.... j.... |H,,,, 1111, || .. 11 u 11 .. I. i H i.,., I.,.. (. I m 111111111II) 1111111H11 h h miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #72972: 1,2-Benzenedicarboxylic acid, bis(trimethysily!) e * * ( • < • i । » > < » l 1 > ' * । * * * । । 147 36.40 36.60 36.80 37.00 73 m/z 207.0 15.29% 5000

45 295 | , , 193 221 119 Tpa Tmmmmmmmppmmmpmpmp • ■ i • • • ■ i ■ ■ ■ ■ i ■ ■ ■ • i ‘ 1 • • i rn/z-> 40 60 80 100120140160180200220240260280300320340360380400420 36.40 36.60 36.80 37.00

30643.D GCMS1126.M Fri Feb 01 10:48:55 2002 Page 17

NYC-WTC_000018467

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NYC-WTC_000018467Source: NYC Law Department, mirrored locally

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