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GCMS analysis results for sample AD31074, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD31074 conducted on January 18, 2002, noting no unusual compounds were detected.

NYC-WTC_000017405–000017433

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0 802\31074.D Vial: 12 Acq On 9 Jan 2002 12:04 am Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 20 Ethanedioic acid, bis(trimethy Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

36.55 0.79 ug/1 120661 Perylene-d12 36.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethanedioioacid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 38 2 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 25 3 3-(3-Hydroxypheny1) -3-hydroxypropio 398 C18H3404S13 000000-00-0 25 4 1,2-Benzenedicarboxylic acid, bis(t 310 C14H2204Si2 002078-22-0 23 Abundance Scan 3432 (36.548 mln): 31074.D (-) m/z 73.00 100.00% 73 147 5000 221 ‘ ‘ I ' ' ' * I * * ’ ' I ‘ TTTTTi 281 355 /on - 55 36 . 96 117 mttnmtpmp 253,1325 ,...........429 111101101101130111101013111110111831153711101/033111 36.20 36.40 36.60 36.80 m/z 147.00 59.20% m/z-> 40 60 80 100120140160180200220240260280300320340 360380400420 Abundance #71006: Ethanedioic acid, bis(trimethylsilyl) ester 73 147 5000 11ftut 36.20 36.40 36.60 36.80 45 m/z 221.0 32.87% 190 219 m/z->__ ha— 117 11।(r..।....!.... ।,... ।।.... ।.... ।. 11. ।.... ।.... ।.... ।.... ।.... ।.... । 40 60 80 100120140160180200220 240260280300320340 360380400420 Abundance 73 147 .0S 36.20 36.40 36.60 36.80 5000 m/z 207.00 16.58% 45 104 193 221 Wt/w m/z->__ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #53668: 3-(3-Hydroxyphenyl)-3-hydroxypropionic add, tri-TMS 73 267 36.20 36.40 36.60 36.80 ‘ *

5000 147

207 398 47 341......... ....... 11293....—11113331111111111111111113331 Tpgpp1111111119111111-1 | m/z-> 40 60 80 100120140160180200220240260280300320340 360380400420 _ 36.20 36.40 36.60 36.80__

31074.D GCMS0103.M Wed Jan 09 12:25:40 2002 Page 20

NYC-WTC_000017432

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NYC-WTC_000017432Source: NYC Law Department, mirrored locally

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