NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\JAN0 802\31074.D Vial: 12
Acq On 9 Jan 2002 12:04 am Operator: 209 GALOS
Sample gems scan 12/20 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 20 Ethanedioic acid, bis(trimethy Concentration Rank 16
R.T. EstConc Area Relative to ISTD R.T.
36.55 0.79 ug/1 120661 Perylene-d12 36.91
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Ethanedioioacid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 38
2 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 25
3 3-(3-Hydroxypheny1) -3-hydroxypropio 398 C18H3404S13 000000-00-0 25
4 1,2-Benzenedicarboxylic acid, bis(t 310 C14H2204Si2 002078-22-0 23
Abundance Scan 3432 (36.548 mln): 31074.D (-) m/z 73.00 100.00%
73
147
5000
221
‘ ‘ I ' ' ' * I * * ’ ' I ‘ TTTTTi
281 355 /on
- 55
36 . 96 117
mttnmtpmp 253,1325 ,...........429
111101101101130111101013111110111831153711101/033111
36.20 36.40 36.60 36.80
m/z 147.00 59.20%
m/z-> 40 60 80 100120140160180200220240260280300320340 360380400420
Abundance #71006: Ethanedioic acid, bis(trimethylsilyl) ester
73
147
5000 11ftut
36.20 36.40 36.60 36.80
45 m/z 221.0 32.87%
190 219
m/z->__ ha— 117
11।(r..।....!.... ।,... ।।.... ।.... ।. 11. ।.... ।.... ।.... ।.... ।.... ।.... ।
40 60 80 100120140160180200220 240260280300320340 360380400420
Abundance
73
147 .0S
36.20 36.40 36.60 36.80
5000 m/z 207.00 16.58%
45
104 193
221
Wt/w
m/z->__ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420
Abundance #53668: 3-(3-Hydroxyphenyl)-3-hydroxypropionic add, tri-TMS
73 267 36.20 36.40 36.60 36.80 ‘
*
5000 147
207 398
47 341......... .......
11293....—11113331111111111111111113331
Tpgpp1111111119111111-1
|
m/z-> 40 60 80 100120140160180200220240260280300320340 360380400420 _ 36.20 36.40 36.60 36.80__
31074.D GCMS0103.M Wed Jan 09 12:25:40 2002 Page 20
NYC-WTC_000017432
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