Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
NYC-WTC_000017703–000017723Folder label: “GCMS X 12/13/01 A 12/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\30425.D Vial: 5 Acq On : 27 Dec 2001 3:04 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T.
34.37 0.52 ug/1 145818 Chrysene-dl2 33.02 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxane, 1,1,1,5,5,5 -hexamethyl 384 C12H3604Si5 003555-47-3 32 2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 25 3 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 23 4 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 23 Abundance Scan 3195 (34.373 min): 30425.D (-) m/z 73.00 1 00.00% 73 147 5000 221 281 355 —mtrTi f. । , tri rr, । < 34.00 34.20 34.40 34.60 34.80
miz-> m 45 ttmpmph , 97 117 —191,+ '"' i'"' i 40 60 80 100120140160180200220240260280300320340360380400420 27 429 yehip m/z 147.00 54.13% Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 .. 5000 ■ ■ i '
281 34.00 34.20 34.40 34.60 34.80 45 369 m/z 221.0, 29.93% 117 207 249 . ________________ 1_____________ BIUIB—304157311" TTTTTTTT TI—TpnnCu8T L111 ’915321100091—3010010130030333101 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #71005: Ethanedioic acid, bis(trimethylsilyi) ester 73
147 34.00 34.20 34.40 34.60 34.80 5000- m/z 281.00 19.99% 45 I il 117 . , 190 219 nnmnammug —mn—mn)—m—apani PPTOITTE)TOICTE]WWTTITNTTOTTETTUTOTTRTT m/z~> 40 60 80 100120140160180200220240260280300320340360380400420 -4—AA4AA A/ ,4448 Abundance #30949: Mercaptoacetic acid, bis(trimethylsilyl)- 73 34.00 34.20 34.40 34.60 34.80 147 m/z 355.0, 15.23% 5000 221 45 193 104 241222224203871 'i1' "i"” i‘ MPgm mmmgpangmgaup ■ I ■ • 1 ' i ‘ ■ miz-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380400420 34.00 34.20 34.40 34.60 34.80
30425.D GCMS1126.M Wed Jan 02 11:04:32 2002 Page 12
NYC-WTC_000017721
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NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017675
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30251 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
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Laboratory report documenting gas chromatography-mass spectrometry reference material analysis conducted on December 31, 2001.
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Laboratory report documenting gas chromatography-mass spectrometry blank analysis conducted on December 27, 2001.
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