NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30352.D Vial: 19
Acq On : 28 Dec 2001 5:38 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C: \HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 14 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 10
R.T. EstConc Area Relative to ISTD R.T.
34.37 1.80 ug/1 508002 Chrysene-dl2 33.02
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 32
2 Ethanedioic acid, Isis (trimethylsily 234 C8H1804Si2 018294-04-7 32
3 2-Hexenedioic acid, bis(trimethylsi 288 C12H24O4Si2 055494-10-5 23
4 Butanoic acid, 3-methyl-2-[ (trimeth 262 C11H2603Si2 055124-92-0 23
Abundance Scan 3195 (34.373 mln): 30352.D (-) m/ z 73.0,0 100.00%
73
5000 147
221
281
45ii ipnS,91117
355
401 429 34.00 34.20 3440 34.60 34.80
tankras । it ii ।. । irp ih । . 11 Eaugman m/z 147.00 46.59%
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet
73
147
5000 ■ i * ■ 1 1 i •
281 34.00 34.20 34.40 34.60 34.80
45 369 m/z 221.05 25.54%
117 4 207 249
T TTTTTpTTTJTTTTpTTTpTTTp-rTrp+TrpTT^^
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance 471006: Ethanodioic acid, bis(trimeth visilyl) ester
73
‘ I ‘ ■ 1 ‘ I 1 ' r ‘ I ' 1 ‘ • • i •
147 34.00 34.20 34.40 34.60 34.80
5000 m/z 281.00 14.74%
45
117 190 219
npmp VpTTTpTTrpTnTrrTTJTTTTJTYTTpTTTJTTTTpn-rTpTTT^^
mfe-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #40777:2-Hexenedioic acid,’ bis(trimethylsilyl) ester, (E)- -+-=-==-=*=
73 34.00 34.20 34.40 34.60 34.80
m/z 355.05 13.11%
5000
147
45
112 244 273
’ ’’l’’I AAS-1A4*414 Trp-rrrp-rrTp-rTTp-rrrylTTrp-nh-pTTTp-rTTp-rrrp-rrrp-rTT^^
i • • > • i ■
m/z—> 40 60 80 100120140160180200220240260280300320340360380400420 34.00 34.20 34.40 34.60 34.80
30352.D GCMS1126.M Wed Jan 02 10:51:12 2002 Page 14
NYC-WTC_000017829
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