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GCMS analysis results for sample AD30352, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.

NYC-WTC_000017808–000017832

Folder label: “GCMS X 12/13/01 A 12/27/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30352.D Vial: 19 Acq On : 28 Dec 2001 5:38 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C: \HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

34.37 1.80 ug/1 508002 Chrysene-dl2 33.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 32 2 Ethanedioic acid, Isis (trimethylsily 234 C8H1804Si2 018294-04-7 32 3 2-Hexenedioic acid, bis(trimethylsi 288 C12H24O4Si2 055494-10-5 23 4 Butanoic acid, 3-methyl-2-[ (trimeth 262 C11H2603Si2 055124-92-0 23 Abundance Scan 3195 (34.373 mln): 30352.D (-) m/ z 73.0,0 100.00% 73

5000 147 221 281 45ii ipnS,91117 355 401 429 34.00 34.20 3440 34.60 34.80 tankras । it ii ।. । irp ih । . 11 Eaugman m/z 147.00 46.59% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147

5000 ■ i * ■ 1 1 i • 281 34.00 34.20 34.40 34.60 34.80 45 369 m/z 221.05 25.54% 117 4 207 249 T TTTTTpTTTJTTTTpTTTpTTTp-rTrp+TrpTT^^ m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance 471006: Ethanodioic acid, bis(trimeth visilyl) ester 73 ‘ I ‘ ■ 1 ‘ I 1 ' r ‘ I ' 1 ‘ • • i • 147 34.00 34.20 34.40 34.60 34.80 5000 m/z 281.00 14.74% 45 117 190 219 npmp VpTTTpTTrpTnTrrTTJTTTTJTYTTpTTTJTTTTpn-rTpTTT^^ mfe-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #40777:2-Hexenedioic acid,’ bis(trimethylsilyl) ester, (E)- -+-=-==-=*= 73 34.00 34.20 34.40 34.60 34.80 m/z 355.05 13.11% 5000 147 45 112 244 273 ’ ’’l’’I AAS-1A4*414 Trp-rrrp-rrTp-rTTp-rrrylTTrp-nh-pTTTp-rTTp-rrrp-rrrp-rTT^^ i • • > • i ■ m/z—> 40 60 80 100120140160180200220240260280300320340360380400420 34.00 34.20 34.40 34.60 34.80

30352.D GCMS1126.M Wed Jan 02 10:51:12 2002 Page 14

NYC-WTC_000017829

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