Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C : \HPCHEM\ 1 \DATA\JAN2 502\30651.D Vial: 35 Acq On : 25 Jan 2002 10:53 pm Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
32.89 1.48 ug/1 862863 Chrysene-dl2 32.80
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 32 2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 3 Butanoic/acid, 3-methyl-2-[(trimeth 262 CllH26O3Si2 055124-92-0 23 4 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 14 Abundance ' ” Scan 3033 (32.891 min): 30651.D (-) m/ z 73.00 100.00% 73
5000 147 221 281 355 32.60 32.80 33.00 33.20 45 98 117 0 11211001111111100111—011111 *914... 249,1... 327 , .. .... 429 111 m 11 rr u p ■ । rp / r i p 111111»p . ।1111 ■ ■ p n t p ri 11 m/z->_____ 40 60 80 100120140160180200220240260280300320340360380400420 m/z 147.00 45.69% Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147
i r । i : i i i it r-r i i । i i 5000 281 32.60 32.80 33.00 33.20 45 369 m/z 221.05 27.78% I , । 117 207 249 TTTTph-rrp-n^rpnTT^ * ' J ' « ' « | « I | I I ' I H I I I >. |> I H 1‘0011009111171111110110111111111111"1117 m/z-> Abundance 40 60 80 100120140160180200220240260280300320340 360380400420 7*006 Ethanedicic ac, isitimothyly yester 73
147 32.60 32.80 33.00 33.20 5000 m/z 281.00 18.85% 45 117 190 219 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #71782: Butanoic acid, 3-methyl-2-[(trimethylsilyl)oxy]-, t ■ ■ । • 1 1 1 11 73 32.60 32.80 33.00 33.20 145 m/z 355.00 18.35% 5000
45 117 , 190 219 247 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 32.60 32.80 33.00 33.20
30651.D GCMS1126.M Mon Jan 28 12:24:07 2002 Page 15
NYC-WTC_000004235
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
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