NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\JAN2502\30651.D Vial: 35
Acq On : 25 Jan 2002 10:53 pm Operator: 209 GALOS
Sample : REINJECT Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
Peak Number 14 1-Monolinoleoylglycerol trimet Concentration Rank 9
R.T. EstConc Area Relative to ISTD R.T.
31.51 1.26 ug/1 736968 Chrysene-dl2 32.80
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 45
2 3-Isopropoxy-1J1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40
3 Butanoic acid, 3-methyl-2-[(trimeth 262 CllH26O3Si2 055124-92-0 32
4 Ethanedioic acid, bis(trimethylsily 234 C8H1804Si2 018294-04-7 32
Abundance Scan 2883 (31.514 min): 30651 .D (-) m/z 73.00 1 00.00%
73
5000 147
221
m/z->
45
' 'I ' 1
50
+-117,4 111914 1 T110
249., . , 327 L
—KmmuTT
401 429
281 355
t.,.v ’"r । ■■■ i । ■ ।
31.20 31.40 3t60 31.80
m/z 147.00 39.36%
'
100 150 200 250 300 350 400 450 500 550
Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether
73
207
5000
147 31.20 31.40 31.60 31.80 '
34 103 ■
281 m/z 221.05 22.68%
> ■ i ■ ■ L ./.335.482.......
m/z-> 50 100 150 200 300 350 400 450
250 500 550
Abundance #60503: 3-isopropoxy-1.1.1,7.7. /-hexamethyl-3,5,5-tris(trim
73
31.20 31.40 31.60 3180 '
5000 m/ z 281.00 15.00%
147
I 221 281 327
I I 415 519 561
m/z--> 50 100 150 200 250 300 350 400 450 500 550
Abundance #71782: Butanoic acid, 3-methyl-2-[(trimethylsilyl)oxy]-, t
73 31.20 31.40 31.60 31.80
145 m/z 355.05 10.73%
5000
45
219 247
■ ' i ' ' —117— । ' '190
tPTTr’ । । .
m/z~> 50 100 150 200 250 300 350 400 450 500 550 31.20 31.40 31.60 31.80
30651.D GCMS1126.M Mon Jan 28 12:24:02 2002 Page 14
NYC-WTC_000004234
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