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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004234
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\JAN2502\30651.D Vial: 35 Acq On : 25 Jan 2002 10:53 pm Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 14 1-Monolinoleoylglycerol trimet Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

31.51 1.26 ug/1 736968 Chrysene-dl2 32.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 45 2 3-Isopropoxy-1J1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 3 Butanoic acid, 3-methyl-2-[(trimeth 262 CllH26O3Si2 055124-92-0 32 4 Ethanedioic acid, bis(trimethylsily 234 C8H1804Si2 018294-04-7 32 Abundance Scan 2883 (31.514 min): 30651 .D (-) m/z 73.00 1 00.00% 73

5000 147 221

m/z-> 45 ' 'I ' 1 50 +-117,4 111914 1 T110 249., . , 327 L —KmmuTT 401 429 281 355 t.,.v ’"r । ■■■ i । ■ । 31.20 31.40 3t60 31.80 m/z 147.00 39.36% '

100 150 200 250 300 350 400 450 500 550 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 31.20 31.40 31.60 31.80 ' 34 103 ■ 281 m/z 221.05 22.68% > ■ i ■ ■ L ./.335.482....... m/z-> 50 100 150 200 300 350 400 450 250 500 550 Abundance #60503: 3-isopropoxy-1.1.1,7.7. /-hexamethyl-3,5,5-tris(trim 73

31.20 31.40 31.60 3180 ' 5000 m/ z 281.00 15.00% 147

I 221 281 327 I I 415 519 561 m/z--> 50 100 150 200 250 300 350 400 450 500 550 Abundance #71782: Butanoic acid, 3-methyl-2-[(trimethylsilyl)oxy]-, t 73 31.20 31.40 31.60 31.80 145 m/z 355.05 10.73% 5000

45 219 247 ■ ' i ' ' —117— । ' '190 tPTTr’ । । . m/z~> 50 100 150 200 250 300 350 400 450 500 550 31.20 31.40 31.60 31.80

30651.D GCMS1126.M Mon Jan 28 12:24:02 2002 Page 14

NYC-WTC_000004234

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NYC-WTC_000004234Source: NYC Law Department, mirrored locally

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