GC/MS calibration data for sample 30643, Dec 2001

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30643.D Vial: 59 Acq On : 30 Dec 2001 5:02 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 1-Monolinoleoylglycerol trimet Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

31.71 2.73 ug/1 1224180 Chrysene-dl2 33.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1 -Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 45 2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 3 3-Isopropoxy- 1,1/1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 30 4 2-Hexenedioic acid, bis(trimethylsi 288 C12H24O4Si2 055494-10-5 23 Abundance Scan 2905 (31.712 min): 30643.D (-) m/ z 73.0,0 100.00% 73

5000 147 221 » » J i i < i J » t < । । s’n i ।' i i > i 281 25E 251... 327. 1 401 429 31.40 31.60 31.80 32.00

m&-> 45 — 50 100 117 +1914 150 200 —— TI***rmftufu!uu*eTnur 250 300350400450500550 m/z 147.00 40.24% Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

207 ------------- 5000 147 31.40 31.60 31.80 32.00 34 103 m/z 221.05 23.03% 281 ___ I _____ t I I _______ 395 482 *j i • • * j k * rn •»•»!’» • ' i 7 ' ' ■ i • ‘ ■ I 1 1 • • i • • miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #30580: Ethanedioic acid, bis(trimethylsilyi) ester 73 147 —. y . 31.40 31.60 31.80 32.00 5000 m/z 281.00 15.27% 45 i ; 190 219 .................. i 1’’’ i । rrf ri i i r I j i i i................. i | i i . i । । । . . , ,1 ,i i. ., . ।. .. ,i i. .. |. ., miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamettiyl-3,5,5-tris(trim . > t . i ‘ । । । । । । . i . . j 73 31.40 31.60 31.80 32.00 m/z 355.05 10.66% 5000 147

m/z-> * i * » * » I ' 50 100 221 281 • i * * * » । > * * » I > » * * । * 150 200 250 300 327, 350 415 a.o* 519 561 400 450 500 550 ...... 1......... IJ I » I »

31.40 31.60 31.80 32.00 » I » » » » I I I < I I ( I t I l'

30643.D GCMS1126.M Fri Feb 01 10:48:36 2002 Page 13

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