Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018470–000018491Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2 701\30645.D Vial: 53 Acq On : 30 Dec 2001 10:14 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 30.25 2.07 ug/1 755989 Chrysene-dl2 33.03 Hit# of 5 Tentati ID MW MolForm CAS# Qual 1 3-Isopropoxy-1, 1,1,7,7,7 -hexamethyl 576 C18H5207Si7 071579-69-6 38 2 1,1,1,5,7,7,7 teptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 33 3 Trisiloxane, 1,1,1,5,5,5 -hexamethyl 384 C12H3604Si5 003555-47-3 16 4 Tris (trijaethylsilyl) borate 278 C9H27BO3Si3 004325-85-3 14 Abundance Scan 2745 (30.245 mln): 30645.D (-) m/ z 73.0.0 100.00% 73
5000 147 221 281 355 m 30.00 30.20 30.40 30.60
m/z-> ' 45 1′1 50 1 ain117. 4, r 11191 100 150__ 200 914—+249. 1327,1 1 401rrts 2S0 300 429 1.... I ■... 1,. 400 3S0 450 500 550 m/z 147.00 36.65% Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73
5000 147 P T 30.00 30.20 30.40 30.60 T
221 281 m/z 221.05 21.47% • ■ i 1 ‘ * I ‘ • i • • ‘ ‘ .327. 415.... 519 561 • i ' ■ m/z->_____ 50 100 150 200 250 300 350 400 450 500 550 Abundance #3671 4:1.1.1.5.7.7.7-Heptamethyl-3.3-bis(Wmethylsitoxy)t 73 T TUT IUT 147 30.00 30.20 30.40 30.60 5000 267 m/z 355.05 13.05% 355 429 45 207 . | ! I . ) . | I I I > | I 1
m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 30.00 30.20 30.40 30.60 281 m/z 281.00 12.35% 5000
369 207 249 338 J.......... 1 1 I ' 1 1 1 1 1 1 ..... .I, m/z-> 50 100 150 200 250'* 366 356 466 456 566 550 * • i 1 ‘ 30,00 30.20 30.40 30.60 ‘ ’ I * ‘
30645.D GCMS1126.M Fri Feb 01 10:53:19 2002 Page 12
NYC-WTC_000018486
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NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
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NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
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Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
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Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
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Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
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Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
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