Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018470–000018491Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\l\DATA\DEC2701\30645.D Vial: 53. Acq On : 30 Dec 2001 10:14 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 N-(Trifluoracetyl)-0,0’,0"-tri Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 28.66 1.45 ug/1 840898 Phenanthrene-dl0 24.98 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N- (Trifluorace, 1)-0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 25 2 Trisiloxane,1 ,1,1,5,5Z5-hexamethyl 384 C12H36O4S15 003555-47-3 17 3 Benzoic acid, :2,5-bis(trimethylsilo 370 C16H30O4S13 003618-20-0 17 4 N-(Trifluoroacetyl)-0,0 ‘,0 ’’-tris(t 481 C19H34F3NO4Si3 000000-00-0 16 Abundance Scan 2572 (28.657 mln): 30645.D (-) m/z 72.9,5 100.00% 73
5000 147 221 281 355 28.40 28.60 28.80 29.00 45 —I ,96 117, 4 , . 1914 k 249 . [ TIT 327, i, 401429 ....... , m/z 147.00 36.78% mfe-> 50 100 150 200 250 300 350 400 ′ 450 500 Abundance #58807: N-(Trifluoracety!)-O,0‘,0"-tris(trimethylsily!)epin 73 355 ......... 5000 1 ' T ' ■ ' I....... 28.40 28.60 28.80 29.00 45 m/z 355.0,5 22.67% ■ ‘i 1 ■ .140 184 ......... 281 ........i................ •480• i i ■ miz-> 50 100 150 200 250 300 350 400 450 500 Abundance #52459; Trisiloxane, 1,1.1,5.5.5-hexametnyl-3,3-bis[(trimet 73 147 ...... .............. 281 28.40 28.60 28.80 29.00 5000 m/z 221.05 22.16% 369 l 4 | , I I | I ! 1 ,1. r 207 249 338 !. miz-> 50 100 150 200 250 300 ' ' 350 400 ‘ 450* ‘ ' 500 — [ A I I I I , I — Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy)-, trimethyls 73 28.40 28.60 28.80 29.00 355 m/z 281.00 17.16% 5000 45
■ • i • ■ • ■ i ■ 147, 179 223, 27,297.. I—r * 1+141*** A t 4 i i | 4 1 . -
m/z-> 50 100 150 200 250 300 350 400 450 500 28.40 28.60 28.80 29.00
30645.D GCMS1126.M Fri Feb 01 10:53:14 2002 Page 11
NYC-WTC_000018485
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NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
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NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
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NYC-WTC_000018417
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
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NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
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NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
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NYC-WTC_000018440
Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
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