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GCMS analysis results for sample AD27232, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD27232 conducted on December 19, 2001.

NYC-WTC_000032847–000032858

Folder label: “GCMS X 11/14/01 A 12/12/01

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Scanned page image, NYC-WTC_000032857
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1201\27232.D Vial: 12 Acq On : 13 Dec 2001 1:18 am Operator: GALOS Sample : gc/ms unknown 11/14 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Benzene, 1-fluoro-3(2-cyanoeth Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

41.60 0.41 ng/uL 82750 Perylene-dl2 37.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzene, 1-fluoro-3(2-cyanoethenyl) 14 7 C9H6FN 000000-00-0 9 2 Benzene, 1-fluoro-4- (2-cyanoethenyl 147 C9H6FN 027530-50-3 9 3 Trisiloxane, 1/1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 9 4 Ethanedioic cid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 9 Abundance 1 Scan 4009 (41.605 min): 27232.D (-) m/ z 73.05 100.00% 73 147

5000 - 221 355 A AA, , 4 281 1 1 11 ' 1 1 1 ' 1 1 I ' ' 1 ' I ' ' 96 429 41.20 41.40 41.60 41.80 42.00 i" ‘' i"' J" " r "' i m/z-> I *"' I mm 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 TTTTTTTTTTTTTIT I i" ■ ‘ i m/z 147.10 72.75% Abundance #9051: Benzene, 1-fluoro-3(2-cyanoethenyl) 147

5000- 120 41.20 41.40 41.60 41.80 42.00 m/z 221. 44.26%

A 75 96 l miz-> I " "i 4 I’UUIIUTETETTTTOETTTTTETITE-TETETTETETETTTTTTTTTTTTETT"T ’’’’I’’’’T 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #9052: Benzene. 1-fluoro-4-(2-cyanoethenyl)-. (E)- 147 ' 1 1 1 1 ' 1 I 41.20 41.40 41.60 41.80 42.00 5000- 120 m/z 354.95 28.69%

75 96 49 T’’’ITTTTTTTTTETEITTTTIT ’TLT | I I I l | • • I l p » I l | . i ’TTTTTTT’TT I | I I I I | I H I | I i l l | I I I I | I i I I | I I I I | I'1 "I m/z-> 40 60 80 100 120 140 160,180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet i ■ ■ ■ ■ i ' ■ |r | ' 73 1 •7 41.20 41.40 41.60 41.80 42.00

281 m/z 281.05 17.48% 5000

m/z-> I ’ "IT’TTTTTTTTTTTTTTTTTTT | I i TIITT । • j .Ti i | 207 249 t TTTTTT , ’I. I,...!..,. I. n . |. I. |... >! > >.. | 40 60 80 100 120 140160 180 200 220 240 260 280 300 320 340 360 380 400 420 338 369 [ Mipuuudnv 41.20 41.40 41.60 41.80 42.00

27232.D NP112701.M Fri Dec 14 10:07:53 2001 Page 3

NYC-WTC_000032857

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