Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\JAN2 502\30651.D Vial: 35 Acq On : 25 Jan 2002 10:53 pm Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 N-(Trifluoracetyl)-O,OO"-tri Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
22.59 2.59 ug/1 2359460 Phenanthrene-dl0 24.78
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 N-(Trifluoracety1)-0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 37 2 N- (Trifluoroacetyl) -0,0',0' '-tris(t 481 C19H34F3NO4Si3 000000-00-0 37 3 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 37 4 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 3 7 Abundance Scan 1911 (22.591 min): 30651 .D (-) m/ z 73.00 100.00% 1 73 1
5000 147 355 221 281 22.20 22.40 22.60 22.80 23.00 45 327 41 441 ... m/z - 117 —96It 191 . 249 .1 147.00 25.30% m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #58807: N-(Trifluoracety)-O,O‘,0"-tris(trimethylsilyl)epin 73 355
5000 22.20 22.40 22.60 22.80 23.00 45 m/z 355.05 23.34% ’’I | 1 , , , , 140 ' I J I I 184,* I I I I I "l 281 , 1 480 ' ' ' i ' m/z-> 50 100 150 200 250 350 400300 450 500 Abundance #58326. N-(Trifluoroacetyh-0.0‘,0"-tris(trimethylsilyl)no 73 355 22.20 22.40 22.60 22.80 23.00 5000 m/z 221.05 17.87%
45 , 126147 .193 265 1376 481 m/z-> 50____ 100 150 200 250 300 350 400 450 500 Abundance #73978: Benzoic acid, 2,5-bis(trimethyisiloxy)-, trimethyls i ■ ■ ■ ' i ' ■ i ' ' ■ ‘ i ' ■ 73 22.20 22.40 22.60 22.80 23.00 355 m/ z 2 81.00 13.65% 5000 45 I TL ......... 147, 179 223, 267 297......... 1 ■ ■ i • ■"1 rru ’ ’ ' i 1 m/z—> 50 100 150 200 250 300 350 400 450 500 22.20 22.40 22.60 22.80 23.00
30651.D GCMS1126.M Mon Jan 28 12:23:34 2002 Page 8
NYC-WTC_000004228
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
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Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
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