Gas chromatography-mass spectrometry analysis of sample AD30936 conducted on 1/28/2002, measuring organic compounds including surrogates and unknown compounds.
NYC-WTC_000018775–000018794Folder label: “GCMS X 12/19/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\JAN2502\30936A.D Vial: 3 Acq On : 25 Jan 2002 11:09 am Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 N-(Trifluoroacetyl)-N,0,0',O'1 Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.
22.60 0.92 ug/1 344908 Phenanthrene-dl0 24.75
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N-(Trifluoroacetyl7-N,0,0',0’'-tetr 553 C22H42F3NO4S14 000000-00-0 43 2 Benzeneethanamine, N- [ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 3 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 37 4 N-(Trifluoro§eetyl)-0,0',0'1-tris(t 481 C19H34F3NO4Si3 000000-00-0 37 Abundance- Scan 1912 (22.596 mln): 30936A.D (-) m/z 73.00 100.00% 73
5000 147 355 ....................................... 221 281 22.20 22.40 22.60 22.80 23.00 ! m/z-> 45 — 50 100 .. 117 191, [ 249. 1 1*ITeT 150 200 3271401 “ 350 ' ‘ 400 ' ' 450 ' 500 ' ' 550 ' 250 300 m/z 147.0,0 24.40% Abundance #60162: N-(Trifluoroacetyl)-N,O,O'.O,’-tetrakis(trimethylsi 73
355 5000- 22.20 22.40 22.60 22.80 23.00 m/z 355.05 20.58% 45 I 147 193 267 538 • • i • • • ‘ | * * * * । > • * * | * < 1 i * * 1 14*5111118 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-K(pentafluoropheny!)methylene] 73 355
22.20 22.40 22.60 22.80 23.00 5000 m/z 221.0,5 17.03%
45 208 251 281 386 458 548 TBDBBBnBG—/BgOGBGDBBOBBOBBBB2BBT0/2.0-m00a0/0//0/1/BB miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy)-, trimethyls 73 22.20 22.40 22.60 22.80 23.00 355 m/z 281.10 12.95% 5000 45 . 147 179 223, 27,297 .. T1 1111111 I I t I miz-> 50166156 266 256 ' 300 350 400 450 500 550 22.20 22.40 22.60 22.80 23.00
30936A.D GCMS1126.M Fri Jan 25 12:24:13 2002 Page 8
NYC-WTC_000018789
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NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018546
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033974
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004149
Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018576
Single-page document containing GCMS data or metadata associated with the WTC site in early January 2002.
Filed in the same folder
NYC-WTC_000018577
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
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NYC-WTC_000018579
Laboratory report documenting GCMS calibration data for sample AD30705 conducted on January 2, 2002.
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NYC-WTC_000018583
Laboratory report documenting GCMS reference analysis of sample AD30705 conducted on January 2, 2002.
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NYC-WTC_000018588
Laboratory report showing non-detect results for volatile organic compounds in a GC/MS blank sample.
Filed in the same folder