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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004229
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2 502\30651.D Vial: 35 Acq On : 25 Jan 2002 10:53 pm Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 9 Phenanthrene-diO Concentration Rank 18

R.T. EstConc Area Relative to ISTD R.T.

24.90 0.23 ug/1 205401 Phenanthrene- dl 0 24.78

Hit# of 5 Teritative ID MW MolForm CAS# Qual

1 Phenanthrene-d10 188 C14D10 001517-22-2 93 2 Pyrrolo[2,/-b]indole, 1,2,3,3a,8,8a 188 C12H16N2 004089-16-1 58 3 Anthracene-d10- 188 C14D10 001719-06-8 52 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 36 Abundance ............ Scan 2163 (24.904 mln): 30651 .D (-) m/ z 18 .10 100.00% 1118

5000

RR 80 94 160

m/z-> 30 42 54 00 | I I I I Tr rttiju ITi | i f I I |'I i 40 50 60 70 80 I T .I 102 118 136 146 | trttm I I I | t TI I | I 1 I I | I I I I | I I 90 100 110 120 130 140 150 160 170 180 190 ,.| 170 180 I I I | I I I I | I I’I" L m/ z 189.10 24.60 24.80 25.00 25.20 17.15% Abundance #19958: Phenanthrene-d10 188

5000 24.60 24.80 25.00 25.20 m/z 8 .05 13.71%

m/z—> ----------- 66 80 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 94 160 Ju Abundance 2 2yirolo,2.3-bingole, i 2.3,3a,3,Sa-hexabydr-3a.8- 144 188

158 24.60 24.80 25'ob 25.20 5000 m/z 184.10 12.84% 130 173 ! TOTumuuuumnupunp—nmmWIWIWDWTWTWTWIITT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188 24.60 24.80 25.00 25.20 ! m/ z . 00 11.95% 5000

66 80 94 J60 | ' ' ■ ■ | ■ ' ■ ■ | ' ■ ■ ■ | • i 1 | > 1 > 11 1 1 >1 | 11 »11 1 1 > > | I 1 1 1 | 1 1 >1 | 1 1 1 > 11 1 i 1 | 1 > I I | r 1 1 1 | 1 1 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 24.60 24.80 25.00 25.20

30651.D GCMS1126.M Mon Jan 28 12:23:39 2002 Page 9

NYC-WTC_000004229

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NYC-WTC_000004229Source: NYC Law Department, mirrored locally

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