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GCMS comments for sample AD26473 detecting N,N-dimethylbenzenesulfonamide

Machine-extracted title · confidence 100%

DEP lab report dated December 10, 2001, identifying N,N-dimethylbenzenesulfonamide at 0.49 ug/L in sample AD26473.

NYC-WTC_000031636–000031649

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26473.D Vial: 9 Acq On : 30 Nov 2001 7:30 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Benzene, pentafluoromethoxy- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 30.58 1.24 ng/uL 427963 Chrysene-dl2 33.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzene, pentafluoromethoxy- 198 C7H3F50 000389-40-2 50 2 Benzene, pentafluoromethoxy- 198 C7H3F5O 000389-40-2 36 3 2-Phenyl-4~/cyanomethyl)-5-methyl-1 198 C11H10N4 013322-20-8 35 4 1,5-Naphthyridine, 2,6-dichloro- 198 C8H4C12N2 027017-66-9 25 Abundance Scan 2807 (30.580 min): 26473.D (-) m/z 91.05 100.00% 91 155 198

5000 45 146 .......... - 65 100 । 212 30.20 30.40 30.60 30.80 31.00 miz—> ,56444477+L... 4 th 30 40 50 60 70 80 90 100110120130140150160170180190200210 m/z 155.00 93.71% Abundance #22177: Benzene, pentafluoromethoxy- 155 198 183 5000 E T T T 117 30.20 30.40 30.60 30.80 31.00 31 m/z 198.05 92.01% 93 105

miz-> Trrrrm-rpT! IIBEI—EAIITIIT .. Mu TTTHg 136 30 40 50 60 70 80 90 100110120130140150160170180190200210 LX i ■" ■ r ■ ■ ■ i Abundance #69575: Benzene, pentafluoromethoxy- 1$5 198 183 3020 30.40 30.60 30.80 31.00 5000 117 m/z 45.1.0 29.43% 93 105

m/z-> —...... .............................................. rr rrp 1111—111111111111101111011211117117 ITT , 136 TTTTTTTHTTIT 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 MMmier i‘"‘i"1‘i Abundance #22325:2-Phenyl-4-(cyanomethy!)-5-methyl-1,2,3-triazole T T T 147 91 30.20 30.40 30.60 30.80 31.00 198 m/z 146.10 28.79% 5000

64 77 51

miz—> TE—IUEITIETEIITTI-IT MJ 1 103 132 172 —00—91—0—091——————— OOO4193431 30 40 50 60 70 80 90 100110120130140150160170180190200210 30.20 30.40 30.60 30.80 3100

26473.D NP112701.M Tue Dec 04 10:45:17 2001 Page 7

NYC-WTC_000031648

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NYC-WTC_000031648Source: NYC Law Department, mirrored locally

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