GCMS comments for sample AD26473 detecting N,N-dimethylbenzenesulfonamide

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26473.D Vial: 9 Acq On : 30 Nov 2001 7:30 pm Operator: GALOS Sample : gc/ms unknown 11/3 InSt : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 6 1-Propanamine, 3-methoxy- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 28.98 1.69 ng/uL 799598 Phenanthrene-dl0 25.19 Hit# of 5 To .tative ID MW MolForm CAS# Qual 1 1-Propanamine, 3-methoxy­ 89 C4H11NO 005332-73-0 35 2 Benzene, 1-[ (2-chloroethyl)sulfonyl 218 C9H11C1O2S 022381-53-9 25 3 2-Butenedioic acid (Z) - 116 C4H404 000110-16-7 25 4 Carbamic acid, [ (4-methylphenyl) sul 257 C11H15NO4S 018303-02-1 16 Abundance Scan 2633 (28.985 min): 26473.D (-) m/z 91.05 100.00% 72 9 45 _ 155 59 5000 199 173

miz-> 1 III , 4 . 20 40 I60 +194116—13% 80 100 120 140 160 2 , 186 180 2i6 229 *' 1 1TTT । I । । r । 200 220 28.60 28.80 29.00 29.20 29.40 m/z 72.05 93.81% Abundance #882:1-Propanamine, 3-methoxy- 33

5000 72 2 28.60 28.80 29.00 29.20 29.40 45 m/z 45.10 66.40% 56 , J, , “•[ — 89 miz-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #27044: Benzene, 1-[(2-chloroethyl)sulfonyl]-4-methyI- 91 155 ' I ' ' • ' i ■ ■ ' ' i ' ' ' ' i ' 1 ' ' i ‘ ' 28,60 28.80 29.00 29.20 29.40 5000 m/z 155.00 61.17% 218 139 190 107 | ----- miz-> Abundance 20

26 40

45 60

72 80 TIBnImUTT 100 120 140 160 ;#3182: 2-Butenedioic acid (Z)- 180 200 220 .... L..... 28.60 28.80 29.00 29'20 29.40 m/z 59.10 58.63% 5000

99 • i • | — 111 1 116..................... ■ i ■ ■ • ■ i ■ ■ ■ ■ i T 1 • ' i • ■ 1 ‘ i ■ ■ m/z—> 20 40 60 80 100 120 140 160 180 20g 220 28.60 28.80 29.00 29.20 29.40

26473.D NP112701.M Tue Dec 04 10:45:16 2001 Page 6

NYC-WTC_000031647