GCMS analysis report for sample AD26393, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26393 .D Vial: 3 Acq On : 30 Nov 2001 2:02 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Benzene-1,2,3,4-d4-, 5,6-dichl Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 11.75 0.54 ng/uL 232174 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzene-1,2, 3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 53 2 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 3 Benzoic acid, 2,5-dimethyl- 150 C9H10O2 000610-72-0 9 4 Biphenylen 152 C12H8 000259-79-0 9 Abundance Scan 753 (11.749 min): 26393.D (-) m/z 150.00 100.00% 150

5000- 115 52 78 1140 11.60 1180 1200 " ' ' mk-> —ht 30 40 50 +340 ’ 11 ■ 1111111.1131 ।।।. 1 । TTT87 60 70 80 90 100 110 120 130 140 150 160 m/z 152.00 60.45% Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150

115 5000 52 78 ---- 11.40 11.60 11.80 12.00 m/z 115.05 41.23% 35 87 ] .. 1.... 1 1... 11 Pp* । ■ i ■ ■ ■ ■ i ■' • ■ i ■ ■ •111''11 ■ ■ 1’11 miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593: 1,4-Dichlorobenzene-d4 150

11.40 11.60 11.80 12.00 5000 115 m/z 78.05 24.97% 52 78

miz-> 30 35 ■ ■ i • ■' ■ i ■ ■ ■ ■ i 40 87 ’111’1-111 1111'> 1111111111111 50 60 70 80 90 100 110 120 +- 130 140 150 160 - Abundance #9719: Benzoic acid, 2,5-dimethyl- T T 104 132 150 11.40 11.60 11.80 12.00 m/z 52.00 , 21.77% 5000 77 51 66 |. - 1 1 11 1 11 I 1 111 11 1 1 • l1 ‘ । ■ I 11 i' ■ • ■ i ■ ■'' i ■ —ITT ■ i' • • * i *1 * • 1111'1 m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.40 11.60 11.80 12.00

26393.D NP112701.M Tue Dec 04 10:43:52 2001 Page 9

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