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GC/MS analysis results for sample AD22550, September 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD22550 conducted on September 27, 2001, identifying unknown compounds.

NYC-WTC_000087044–000087058

Folder label: “508 Scan 9/18/01 9/27/01

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Scanned page image, NYC-WTC_000087056
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\l\DATA\SEP2601\22550.D Vial: 4 Acq On : 26 Sep 2001 1:12 pm Operator: GALOS Sample : GC/MS unknown Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\DAT7kBASE\NBS75K.L ********************************************************************* Peak Number 5 Benzene-1,2,3,4-d4-, 5,6-dichl Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 11.85 0.43 ng/uL 64339 1,4-Dichlorobenzene-d4 12.00 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 2 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 9 4 Benzenamine, 2-methyl-5-nitro- 152 C7H8N202 _______000099-55-8 9 Abundance Scan 765 (11.849 min): 22550. D (-) m/z 150.00 100.00% 1$0

5000 115 52 78 11.60 11.80 12.00 12.20 40 87 I m/z 152.00 67.34% ' ' I ‘ ' 'I' ' ' ' I ' ' ' I ' ’ ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' i ' ' Ti^-> Abundance 30 40 50 '' sb" 70 80 90 100 110 120 130 140 150 160 #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1!i0 ft 115 5000 52 78 I ' ' ' ‘ I ' ' 11.60 11.80 12.00 12.20 m/z 115.05 42.31% 35 87 I I ........ m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1!i0

' I'''' I'' 11.60 11.80 12.00 12.20 5000 115 m/z 78.05 29.01% 52 78

35 mlz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 ZXbundance #66892: Benzaldehyde, 2-hydroxy-3-melhoxy- 1!I2 11.60 11.80 12.00 12.20 Wz 52.10 26.82% 106 5000 53 81

122 '' I' ''' I' ' ' ' I ' 136 ' I '' ' ' I ' ' ' ' I I ''I' m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.60 11.80 12.00 12.20

22550.D NP072501.M Mon Oct 01 14:37:05 2001 Page 5

NYC-WTC_000087056

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NYC-WTC_000087056Source: NYC Law Department, mirrored locally

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