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GC/MS analysis results for sample AD22558, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22558 conducted on October 1, 2001, identifying unknown compounds.

NYC-WTC_000087097–000087119

Folder label: “508 Scan 9/18/01 9/27/01

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Scanned page image, NYC-WTC_000087109
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2701\22558.D Vial: 2 Acq On : 27 Sep 2001 1:02 pm Operator: GALOS ■ Sample : gc/ms unknown <1 ml Inst : GC/MS Ins Mise : Multiplr; 1,00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Benzene-1,2,3,4-d4-, 5,6-dichl Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 11.83 .0.44 ng/uL 67506 1,4-Dichlorobenzene-d4 11.97 Hit# of Tentative ID MW MolForm CAS# Qual

1 Benz^e-l,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 45 2 1,4-^ichlorobenzene-d4 150 C6C12D4 003855-82-1 36 3 Bip/enylene 152 C12H8 000259-79-0 9 4 Be/zaldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 9 fiibund^e Scan 763 (11.831 min); 22558. D {-) m/z 150.00 100.00% 1$0

5000 115 52 78 40 11.40 11,60 11.80 12.00 12.20

■nZz-> 30 Ui RU. m/z 152.00 40 50 60 70 80 90 100 110 120 130 140 150 160 1 65.28% Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1!i0

552 52 78 115 R ^“1 '

11.40 11.60 11.80 12.00 12.20 m/z 115.05 43.12% 35 87 ' I'''' I'' (' I yJJn- ... ■n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 liiO

11.40 11.60 11.80 12.00 12.20 5000 115 m/z 52.10 27.06% 52 78

35 UUn .p^X****,^^ m/z-> Abundance 30 40 50 60 70 80 90 100 #67017: Biphenylene 110 120 130 140 150

152 160 T 11.40 11.60 11.80 12.00 12.20 m/z 77.95 A, 25.61%

5000

63 76

'' I' Ti/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.40 11.60 11.80 12.00 12.20

22558.D NP072501.M Mon Oct 01 14:52:21 2001 Page 5

NYC-WTC_000087109

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NYC-WTC_000087109Source: NYC Law Department, mirrored locally

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