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GC/MS analysis results for sample AD22558, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22558 conducted on October 1, 2001, identifying unknown compounds.

NYC-WTC_000087097–000087119

Folder label: “508 Scan 9/18/01 9/27/01

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Scanned page image, NYC-WTC_000087110
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2701\22558.D Vial: 2 Acq On : 27 Sep 2001 1:02 pm Operator: GTkLOS ■ Sample : gc/ms unknown <1 ml Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\DATABASE\NBS75K.L ********************************************************************** Peak Number 6 Cyclopentanecarboxylic acid, 2 Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 29.69 1.00 ng/uL 133308 Chrysene-dl2 33.29 Hit# of 5. Tentative ID MW MolForm CAS# Qual

1 Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2; 040482-05-1 37 2 Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2; ' 037910-65-9 37 3 Pip^idin-4-carboxylic acid 129 C6H11NO2 000498-94-2 25 4 2-r^thyl-N-1-tridecene 196 C14H28 018094-01-4 25 ^bundai Scan 2710 (29.685 min): 22558.D (-) Wz 56.10 100.00% 5

41 73 1OQ 257 29.40 29.60 29.80 30.00 11 III .g i?’T......... ? I m7z 57710 49.98% Tife-> Abundance 20 40 60 80 100 120 140 160 #5212: Cyclopentanecarboxylic acid, 2-amino-, trans- 180 200 220 240 260 J 53

A-TT-r-r-.- 5000 29^40 29:60 29.80 30.00 m/z 41.10 39.06% 30 69 82 100 129 ,1 42 |l| ,l, . , , I................. ,l| I I I I I I I i-i-i I I I I I , I I I I I I I.................................

TiZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #5218: Cyclopentanecarboxylic acid, 2-amino-, cis-

'' I'' 29.40 29.60 29.80 30.00 5000 m/z 43.10 37.85%

30 69 82 100 ,1 42 ........................... ^z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #5228: Piperidin-4-carboxylic acid 5|5 29.40 29.60 29.80 30.00 m/z 55710 28.70%

5000

•n/z-> ux 20 42

40 60 84

80 I 100 100 ,,1. . .. . . . 120 140 160 180 200 220 240' ' 260 29,40 29.60 29.80 30.00

22558.D NP072501.M Mon Oct 01 14:52:24 2001 Page 6

NYC-WTC_d000871ld

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NYC-WTC_000087110Source: NYC Law Department, mirrored locally

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