GCMS analysis report for sample AD26392, Dec 2001

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DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26392 noting other unknown compounds.

NYC-WTC_000031530–000031549

Folder label: “GCMS X 11/5/01 A 12/1/01”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26392 .D Vial: 5 Acq On : 30 Nov 2001 3:52 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise ! Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method ; C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 1,4-Dichlorobenzene-d4 Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 11.74 0.56 ng/uL 245527 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlor©benzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-12,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 53 3 Biphenylene 152 C12H8 000259-79-0 9 4 Benzoic acid, 2,5-dimethyl-_______150 C9H10O2 000610-72-0 9 Abundance Scan 753 (11.744 min): 26392.D (-) m/z 150.00 100.00% 150

5000 115 52 78 -------

miz-> - 40

30 40 50 ++ 60 87 । i. III ■ 70 80 90 100 110 120 A 130 140 I— — 150 160 11.40 11.60 11.80 12.00 m/z 152.00 64.43% Abundance #9593:1,4-Dichlorobenzene-d4 150

115 __। i_________ — / I • • ■ • I • • rr । । । . i . . । . 50)0 78 11.40 11.60 11.80 12.00 52 m/z 115.05 42.13%

mlz-> 30 35 TT ; , i i n-rrn-j- " ' I " " I " 40 50 60 70 87 -PPP +- 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 —...........- — 115 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 23.30%

35 87 - -n-p-n-r-p-T _...... i •' * ‘ i • > * • i *1 l‘. | | 1— miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 180 Abundance #67017: Biphenylene J "-11/-1/11/1/1/1/11/1/1/111/1/1/1///1/T 152 11.40 11.60 11.80 12.00 m/z 52.00 21.55% 5000

63 76 126 .................... .1....... 97 TI—I— u—— tuTr1 TITIT ■ ‘’I TIIT ______________________ ■ ■ i 4 '■■ i ' ' rTi r' ' 1 i ' ''‘ i ' m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.40 11.60 11.80 12.00

26392.D NP112701.M Tue Dec 04 10:43:14 2001 Page 11

NYC-WTC_000031548

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GCMS analysis report for sample AD26393, Dec 2001 · Box DEP Box 21

NYC-WTC_000031550

DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26393 noting other unknown compounds.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999