Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
NYC-WTC_000036614–000036644Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File C:\HPCHEM\1\DATA\JAN0802\29466.D Vial: 6 Acq On 8 J an 2 002 5:14 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K. L ********************************************************************* Peak Number 16 1-Monolinoleoylglycerol trimet Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
35.42 22.01 ug/1 4782530 Perylene-dl2 36.91
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1-Monolinoledylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 39 2 Ethanedioic/acid, bis(trimethylsily 234 C8H1804Si2 018294-04-7 25 3 N-Benzhydrylidene-1- (2,4,6-trimethy 343 C24H25NO 089839-57-6 22 4 2-Propenoic acid, 2-[(trimethylsily 232 C9H20O3Si2 055191-13-4 17 'Abundance Scan 3309 (35.424 min): 29466.D (-) m/ Z 73.0^100.00% 73
147 5000 221 281 355 35'00 35.20 35.40 35.60 35.80 45 Tid 96 117 . .... . —4-249 4—443274 401 4 m/z 147.00 54.47% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73
207 5000 147 | ■ ■ ■ > i • •
35.00 35.20 35.40 35.60 35.30 34 103 281 m/z 221.05 34.71% AL , 325 482 miz-> 50 100 150 200 250 300 350 400 450 Abundance #71006: Ethanedioic acid. bis(trimethylsily!) ester 73 ■ i ■ ■ 1 ' i ■ ' 147 35.00 35.20 35.40 35.60 35.80 5000 m/z 281.0,0 19.57% i I
45 I : 117 | 190 219 m/z-> 50 100 150 200 250 300 350 400 450 Abundance #48514: N-Benzhydrylidene-1 -(2,4,6-trimethylphenyl)ethylami ) । i T1 ■ ‘ ' 1 1 ‘ 147 35.00 35.20 35.40 35.60 35.80 m/z 355.05 16.56% 5000
................. 182 ...................... 312 343 ................... T II" m/z—> 50 100 150 200 250 300 350 400 450 35.00 35.20 35.40 35.60 35.80
V
29466.D GCMS0103.M Wed Jan 09 16:17:06 2002 Page 16
NYC-WTC_000036639
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NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033974
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018287
Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000036491
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036492
Fragmented page from a DEP environmental sampling record containing partial text and data fields.
Filed in the same folder
NYC-WTC_000036494
Laboratory calibration data sheet for GCMS analysis of organic compounds including nitrosamines and chlorobenzenes dated December 13, 2001.
Filed in the same folder
NYC-WTC_000036498
Laboratory report detailing GCMS calibration analysis for various organic compounds including nitrosamines and chlorobenzenes conducted on December 13, 2001.
Filed in the same folder
NYC-WTC_000036503
Laboratory report documenting GCMS blank analysis for organic compounds conducted on January 4, 2002, showing results below detection limits.
Filed in the same folder