GCMS sample results, AE00918, Feb 26, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1102\918.D Vial: 39 Acq On : 13 Feb 2002 1:07 am Operator: 209 GALOS Sample : GC/MS SCAN 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Bis(2-ethylhexyl) phthalate Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

34.03 0.30 ug/1 20991 Chrysene-dl2 33.82

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Bis (2-ethylhexyl) phthalate ” 390 C24H3804 000117-81-7 78 2 1,2 -Benzenedi ealluxyHi c acid? 3-nit 211 C8H5NO6 000603-11-2 64 3 1,2-Benzenedicarboxylic acid, diiso 390 C24H3804 027554-26-3 58 4 Di-n-octyl phthalate 390 C24H3804 _ 000117-84-0 47 Abundance Scan 3157 (34.027 min): 918.D (-) m/z 14 9. 0.0 10 0. 00% 149

5000 57 167 41 70 1 II 83 104 207 279 33.60 33.80 34.00 34.20 34.40 — ■' 'I' I ■ w ■ 3 ■ ■ I__ L i m/z 57.00 32.41% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #53128: Bis(2-ethylhexyl) phthalate 149

5000 i 1 * ‘ । ■ *- * r * ■ > ■ i * ■ 57 167 33.60 33.80 34.00 34.20 34.40 71 m/z 167.00 32.25% ! || 83 113 ' 1 I 1 1 1 । I 1 11 111i .1/132 1—11———PWP0T1TT 279 m/z->40 60. 80 100 120 140 160 180 200 220 240 260 280 Abundance 149 1 । > 11111 1’*’I 33.60 33.80 34.00 34.20 34.40 5000 m/z 41.05 23.45% 167 71 83 113 132 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #53134:1,2-Benzenedicarboxylic acid, diisooctyl ester T 1tT 149 33.60 33.80 34.00 34.20 34.40 m/z 43.05 23.22% 5000- 57 70 167

. 83 104 121132 279 111 ■ ■ ■11 ■ ■1 ■ । ■ • i ■ ................. 1 ‘ ‘ l ■ • ‘ 1 1 1 1 1 I 1 1 ' 1 1 1 1 1 1 ! 1 ' 1 1 1 1 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 i ■ ■ ■ ■ i ' ' ‘ ‘ i ■ ' ■ ■ i • ' 33.60 33.80 34.00 34.20 34.40

918.D GCMS0208.M Wed Feb 20 09:55:23 2002 Page 1

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