GCMS unknown compounds report, sample AD31501, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1802\31501.D Vial: 11 Acq On : 19 Jan 2002 1:22 am Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.27 1.00 ug/1 261351 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2 -Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Propanol/ 1,1' -oxybis- 134 C6H14O3 000110-98-5 50 3 Ethane, 1-ethoxy-1-methoxy- 104 C5H12O2 010471-14-4 45 4 1 - Propanol , 2 - (2 - hydroxypropoxy) - 134 C6H14O3 000106-62-7 42 Abundance “ "Scan 678 (11.266 min): 31501.D (-) m/z 59.05 100.00% 59

5000

--l-514 45

.8084... 1.. . 73 103 Ml 11.00 11,20 11.40 11,60 m/ z 45.05 54.63% Ti

m/z-> 20 30 40 50 60 70 90 100 110 120 130 __ Abundance #9238:2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 103 ■ ■ i ■ ■ 45 73 11.00 11.20 11.40 11.60 31 m/z 103.00 30.90% ------- mm __________ .__________ 130 • i ■ ■ • ■ i ■ ■ ■ ■ i • ‘ ' i ' ■ • ■ i ‘ 11 1 1 mtz-> 20 30 40 50 _ 60 70 80 90 100 110 120 130 Abundance 42087 -5D, ant ; : yH 59 TTPri • ■ i r■ ■ • i ■ ■ ■ • i 11.00 11.20 11.40 11.60 31 5000 45 m/z 41.05 27.36% 103 89 72 ■ i • ■ • • i • ■■■i1•i■ 1 ■ ■ I ‘ 1 • ■ i ■ ■ ■ • i ■ ■ ■ ■ i ■‘■i■■■■i■ ■ ■ ■ i ■ ■ ■ ' i ■ miz-> 20 30 40 50 60 70 80 90 100 110 120 130 (Abundance #1926: Ethane, 1-ethoxy-1-methoxy- 59 45 m/z 73.00 25.77%

m/z-> 5000

) 20 30 27

40 l ' '50I ' 1 — 60 ________ 73 89

103—_______________ *1/2////n////n//n//t/Bn/B 70 80 /B/B—B3B/B/B/nB——/Sn/B.n 90 100 110 120 130 I 11.00 11.20 11.40 11.60

31501.D GCMS0103.M Wed Feb 06 15:35:49 2002 Page 4

NYC-WTC_000016623