GCMS analysis report for sample AD26433, Dec 2001

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Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV3001\26433 .D Vial: 21 Acq On 1 Dec 2001 6:24 am Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.75 0.52 ng/uL 253319 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 entative ID MW MolForm CAS# Qual 1 1,4-Dichl obenzene-d4 150 C6C12D4 003855-82-1 96 2 Benzene- ,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 42 3 Benzald hyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 35 4 2H-1-B zopyran-3-ol, 3,4-dihydro- 150 C9H10O2 021834-60-6 9 Abundance Scan 753 (11.750 min): 26433.D (-) m/z 150.00 100.00% 150

5000 115 78 ■ i-| । i > । — — । — । r 52 40 11.40 11.60 11.80 12.00 ’ 1 -1 —70—11“ 87 nuur 1 L m/z 152.00 64.48% mlz-> 30 40 50 60 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 52 78 115 ■ ■ i ■ ■ • ■ i ■ ■ A 11.40 11.60 11.80 12.00 m/z 115.05 41.58% 35 87 ■ • । ■ i * • > * । ‘ '111 11 11 1 ' P 1 । | ■ > । । |T> 1 > | • । 1 1 1 ' miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 '11.40 1—P ----- 11.60 11.80 12,00 115 5000- 52 78 m/z 78.05 22.56%

35 87 I I 111’111111111 ■ i ‘ ‘ ‘ ‘ i ' ' — Im i • •' • i ■ ‘ miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 152 111/11/1/11/1.7 11.40 11.60 11.80 1200 A m/z 52.10 21.38% 106 5000- 53 81

- 92 122 — 136 - — -PP • • । • i • • • > j» 1111111 1128 ‘ i •'' ■ i ' ■' i' m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 | 11.40 11.60 11.80 12.00

26433.D NP112701.M Tue Dec 04 15:08:14 2001 Page 4

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