GCMS analysis results for sample AD26321, Dec 2001

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Library Search Compound Report Data File : C: \HPCHEM\ 1 \DATA\NOV3 001\26321.D Vial: 31 Acq On : 1 Dec 2001 3:30 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Oxirane, 2,2-dimethyl-3-propyl Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 10.32 0.70 ng/uL 211211 1,4-Dichlorobenzene-d4 11.88 Hit# of 5 tentative ID MW MolForm CAS# Qual 1 Oxirane, 2, 2-dimethyl-3-propyl- 114 C7H140 017612-35-0 17 2 Oxirane,/2-methyl-3-propyl-, cis- 100 C6H120 006124-90-9 12 3 1-Butanol, 4- (1-methylethoxy) - 132 C7H1602 031600-69-8 12 4 Pyrrolidine, 3-methyl- 85 C5H11N 034375-89-8 10 Abundance Scan 597 (10.316 min): 26321.D (-) m/z 43.10 100.00% 43

5000 55

73 85 r rn r +/ ■ NP 10.00 10,20 10.40 10.60

miz-> — 3+4 Tpo 30 35 40 45 50 55 60 65 70 75 80 85 90 .................. 100 -rp-rrr .. 11111.. 11..11.. 11J. 11111111111111111 100 105110 115 120 m/z 55.10 44.25% Abundance #3003: Oxirane, 2,2-dimethyl-3-propyl- 43 59 85

5000- ‘11/1/1/111/8." A... 10.00 10.20 10.40 10.60 72 m/z 59.10 39.18% 11 ‘ ‘ ” ।" * •! — “i1 ” ■ i1 ‘11 ।...(.i।11.... ।1111p1“ 111111j “ । -114 nfe-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 115 120 Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- 43 -................. —

57 10.00 10.20 10.40 10.60 5000 71 85 m/ z 57.10 36.06%

100 m/z-> r30..... mill ■ i■■ ■ ■i • ■■ ■ i 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 120 T1—113 II.... I.... 1.111111 > IJ >■ 111 > 11

Abundance 43 #5820:1-Butanol, 4-(1-methylethoxy)- a-- 1 ' f111 *I 10.00 10,20 10.40 10,60 m/z 41.10 32.43% 55 73 5000

89

m/z—> ■ i ■“ ■ i ■ i" ’’11111 + 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110115 120 'i1'" i""i 1“ “ I 102 i11" i t »■»■> > j > • • • i 1A,AA-A-4 -A L MM 4 10.00 10.20 10.40 10.60 1

26321.D NP112701.M Tue Dec 04 10:13:30 2001 Page 5

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