GCMS analysis results for sample AD26676, Dec 10 2001

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 6 01\26676.D Vial: 9 Acq On 6 Dec 2001 5:28 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Oxirane, 2,2-dimethyl-3-propyl Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

10.31 548910 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxirane, 2,2-dimethyl-3-propyl- 114 C7H140 017612-35-0 17 2 Pyrrolidine, 3-methyl- 85 C5H11N 034375-89-8 14 3 CH2=CHCH2C(0)OCH3 100 C5H802 003724-55-8 14 4 Oxirane, 2-methyl-3-propyl - , cis- 100 C6H120 006124-90-9 12 Abundance Scan 597 (10 314 min): 26676.D (-) m/z 43.05 100.00% 1 4b

5000 59

73 85 10.00 10.20 10.40 10.60 I ■ ■ i ' ' ■ ■ i ■ ■ ■ ■ i ' +384 .. ... ' —l ' l ' —. 100. — m/z 59.10 42.71% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 'Abundance #3003: Oxirane, 2,2-dimethyl-3-propyl- 43 59 85

5000- -- ----- 10.00 10.20 10.40 10.60 72 m/z 55.10 38.25% — 99 114 ' ' . .......... ■ i ' ■ ■ ■ i 1 • > i ■ ■ ---------- m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #637: Pyrrolidine, 3-methyl- 43 ----- 4 । r ... । 10.00 10.20 10.40 10.60 5000 - m/ z 33.90% 85 57.10 15 27 56 68 • > i • • ■ 1 I > • i ■ ■ • ■ । ■ i ■

-----A 1 ■ ' i ■ ■ ' ■ i ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #1448: CH2=CHCH2C(O)OCH3 4 10.00 10.20 10.40 10.60 m/z 41 - 10 32.09% 5000

58 ....................... 38 72 100 ’ 1 I 1 ' ' ' I ' ' ' 1 I ' ' ' ' I 1 ■ • i ■ ■ > । i • -H— — — PPT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 10.00 10.20 10.40 10.60

26676.D NP112701.M Fri Dec 07 14:51:40 2001 Page 10

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