GCMS analysis results for sample AD26681, Dec 10 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0401\26681.D Vial: 2 Acq On 4 Dec 2001 11:44 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Oxirane, 2-butyl-3-methyl-, ci Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

10.30 0.68 ng/uL 287135 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxirane, 2-butyl-3-methyl- , cis- 114 C7H140 056052-93-8 25 2 Oxirane, 2,methyl-3-propyl-, cis- 100 C6H120 006124-90-9 12 3 Ether, 3-butenyl propyl 114 C7H140 034061-75-1 12 4 Oxirane, 2,2-dimethyl-3-propyl- 114 C7H140 _________ 017612-35-0 12 'Abundance Z Scan 595 (10.301 min): 26681.D (-) m/z 43.0.5 100.00% 43 A

5000 59 73 85 TTT iI ....... 36 I ■+ . I .... I .... i 53 | ' ■ ' 1 i ■ ■ ' ■ _ i 1 • 1 100 ' I ■ ' ' ' I ' ‘ ' I ' 10.00 10.20 10.40 10.60 m/z 59.10 38.65% mlz-> 20 30 40 50 60 70 80 90 100 110 120 'Abundance #3063: Oxirane, 2-butyl-3-methyl-, cis- 4

5000 55 71 85 1 1A ' —mr ' 1 i 10.00 10.20 10.40 10.60 m/z 55.10 34.33% ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i • ■ i ’ • , 1 —... , A 114 , ! , miz-> 20 30 40 50 70 60 80 90 100 110 120 'Abundance #1531: Oxirane, 2-methyl-3-propyl-. cis- 43 4—A 10.00 10.20 10.40 10.60 57 5000 71 85 m/z 57.10 31.87% I I ' I1! m/z-> Abundance । ' I ' ' ' ' i ' ' ' ' i ' ' 20 30 40 43 50 Di 60 70 #3059: Ether, 3-butenyl propyl 80 90 100 110 120 _.. _A 10.00 10.20 10.40 10.60 ‘I

m/z 41.10 31.16% 5000

55 73 85

1 1 """U 30 । I Tki 1 1 1 *1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 10.00 10.20 10.40 10.60

26681.D NP112701.M Fri Dec 07 13:12:33 2001 Page 7

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